Prince:Mass Spectrometry

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Contents

Sample Preparation

Proven Methods:

Side Notes:

Equipment

Gases

[From the wall out]

  • Helium UHP [LTQ] (40psi)
  • Nitrogen UHP [HCD] (100psi)
  • Nitrogen 99% (this is the normal nitrogen in the stock room) [sheath & Orbitrap bath] (100psi)
  • Nitrogen? Normal? psi? [for UPLC]

UPLC

  • UPLC (Fittings/tubing/flow rates)

Tuning/Calibration

Mascot Restart

 user@jp1:~$ ls /etc/init.d/mascot
/etc/init.d/mascot
user@jp1:~$ sudo /etc/init.d/mascot status
[sudo] password for user:
user@jp1:~$ sudo /etc/init.d/mascot restart
 * Mascot monitor is not running
 * Mascot monitor started
user@jp1:~$
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