From OpenWetWare
(Difference between revisions)
|
|
| (8 intermediate revisions not shown.) |
| Line 1: |
Line 1: |
| - | ==General Lab Protocols==
| + | {{deleteme}} |
| - | | + | test |
| - | Will need to split this page up with daughter pages
| + | |
| - | | + | |
| - | [[Standard metal salts to try for cyclam complex crystallisation]]
| + | |
| - | Typical add-ins are PF6-, BF4-, Ph4B-, Cl4Zn2-. Usually use MeOH or MeCN as solvents for these.
| + | |
| - | | + | |
| - | Typical mixed-solvent diffusion tank methods are to dissolve the sample in MeCN, acetone, DMF or MeOH and allow ether to diffuse in.
| + | |
| - | | + | |
| - | Typical metals (generally) for cyclam recrysts are Cd, Ag (dark), Hg or Pb (usually sit on azamacrocycle, rather than in it). Fe(II)(BF4-)2 in MeCN is good.
| + | |
Current revision
| It has been requested that this page be removed with restriction endonucleases.
Other articles for deletion are listed here.
|
test
