User:Abigail E. Miller/Notebook/MOF Project/2013/01/23

Current revision

Metal Organic Frameworks

9am removed DO2A plus zinc reaction from the solution
- yellowish solution with white suspension
- white solid material on bottom and sides of vial
- let cool to room temp on the bench t

also removed PPF18 and PPF18A samples from powder XRD
- sensor, went off due to over heating of the X ray source

exchanging DPNI for adenine
- mixed 0.5 mL of ethanol and 1.5 mL DEF
- added 0.0070 mg adenine, but it did not all dissolve
- collected UVVis spectrum of solution

Weight of PPF18
- paper 0.1332 g
- paper plus PPF18 0.1528 g
- after putting in 10mL beaker, paper 0.1332 g
- Some loss of material to static

1:30 pm filtered PPF18 with adenine
- filtrate was purple - indicates presence of porphyrin, dissolved from the PPf18
- washed with DEF

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 ==Objective==
-* Insert content here...
+* exchange DPNI for adenine in PPF-18 (PPF-18A)
+* powder XRD of PPF-18A
+* filter, collect and powder XRD of attempt to synthesis MOF with DO2A
 ==Bench Work==
-* Insert content here...
+* 9am removed DO2A plus zinc reaction from the  solution
+** yellowish solution with white suspension
+** white solid material on bottom and sides of vial
+** let cool to room temp on the bench t
+* also removed PPF18 and PPF18A samples from powder XRD
+** sensor, went off due to over heating of the X ray source
+* exchanging DPNI for adenine
+** mixed 0.5 mL of ethanol and 1.5 mL DEF
+** added 0.0070 mg adenine, but it did not all dissolve
+** collected UVVis spectrum of solution
+*Weight of PPF18
+** paper 0.1332 g
+**paper plus PPF18 0.1528 g
+** after putting in 10mL beaker, paper 0.1332 g
+**Some loss of material to static
+* 10:20am added 1mL of adenine solution to PPF18
+** waiting 3 hrs
+* filtered material from DO2A and zinc reaction
+* 1:30 pm filtered PPF18 with adenine
+** filtrate was purple - indicates presence of porphyrin, dissolved from the PPf18
+** washed with DEF
 ==Data/Spectra==