User:Abigail E. Miller/Notebook/MOF Project/2013/01/23: Difference between revisions

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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Metal Organic Frameworks</span>
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Metal Organic Frameworks</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
|style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}}
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==Bench Work==
==Bench Work==
* Insert content here...
* 9am removed DO2A plus zinc reaction from the  solution
** yellowish solution with white suspension
** white solid material on bottom and sides of vial
** let cool to room temp on the bench t
 
* also removed PPF18 and PPF18A samples from powder XRD
** sensor, went off due to over heating of the X ray source
 
* exchanging DPNI for adenine
** mixed 0.5 mL of ethanol and 1.5 mL DEF
** added 0.0070 mg adenine, but it did not all dissolve
** collected UVVis spectrum of solution
 
*Weight of PPF18
** paper 0.1332 g
**paper plus PPF18 0.1528 g
** after putting in 10mL beaker, paper 0.1332 g
**Some loss of material to static
 
* 10:20am added 1mL of adenine solution to PPF18
** waiting 3 hrs
 
* filtered material from DO2A and zinc reaction
 
* 1:30 pm filtered PPF18 with adenine
** filtrate was purple - indicates presence of porphyrin, dissolved from the PPf18
** washed with DEF


==Data/Spectra==
==Data/Spectra==

Latest revision as of 22:22, 26 September 2017

Metal Organic Frameworks Main project page
Previous entry      Next entry

Objective

  • exchange DPNI for adenine in PPF-18 (PPF-18A)
  • powder XRD of PPF-18A
  • filter, collect and powder XRD of attempt to synthesis MOF with DO2A

Bench Work

  • 9am removed DO2A plus zinc reaction from the solution
    • yellowish solution with white suspension
    • white solid material on bottom and sides of vial
    • let cool to room temp on the bench t
  • also removed PPF18 and PPF18A samples from powder XRD
    • sensor, went off due to over heating of the X ray source
  • exchanging DPNI for adenine
    • mixed 0.5 mL of ethanol and 1.5 mL DEF
    • added 0.0070 mg adenine, but it did not all dissolve
    • collected UVVis spectrum of solution
  • Weight of PPF18
    • paper 0.1332 g
    • paper plus PPF18 0.1528 g
    • after putting in 10mL beaker, paper 0.1332 g
    • Some loss of material to static
  • 10:20am added 1mL of adenine solution to PPF18
    • waiting 3 hrs
  • filtered material from DO2A and zinc reaction
  • 1:30 pm filtered PPF18 with adenine
    • filtrate was purple - indicates presence of porphyrin, dissolved from the PPf18
    • washed with DEF

Data/Spectra

  • Insert content here...

Notes

  • Insert content here...


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