User:Abigail E. Miller/Notebook/MOF Project/2013/01/25: Difference between revisions

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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Metal Organic Frameworks</span>
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Metal Organic Frameworks</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
|style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}}
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==Bench Work==
==Bench Work==
* Insert content here...
====exchanging PPF-18 with guanine and adenine====
*
 
====synthesizing PPF-18 and PPF-20====
* Added zinc nitrate hexahydrate, DPNI and TCPP to four vials.
** insert chart with weights here
 
*added 1.75 mL of leftover 75% DEF/25% EtOH to vials 1-3, 1 mL in vial 4
** made a fresh solution of 75% DEF/25% EtOH and added 1mL to vial 4
** added 250 μL of pure ethanol to vials 1-3
 
*made a 10 mL solution of 1 M nitric acid in ethanol
** 10 mL * 1 M = x mL * 15. 8M --> x= 1.58 mL conc nitric acid
** --> added 1.58 mL of conc nitric acid to 8.46 mL of ethanol
 
* added 100 μL of 1M HNO3 in EtOH to vials 1&2 and 80 μL to vials 3&4
 
* sonciated vials and placed in oven at 3pm
** programmed to heat at 80 °C for 24 hrs then cool to 0 °C (20 °Croom temp) over 9 hrs


==Data/Spectra==
==Data/Spectra==

Latest revision as of 22:23, 26 September 2017

Metal Organic Frameworks Main project page
Previous entry      Next entry

Objective

  • Synthesis of PPF18 and PPF20
  • exchange PPf18 with adenine and guanine
  • make a stock solution of 1M HNO3 in ethanol

Bench Work

exchanging PPF-18 with guanine and adenine

synthesizing PPF-18 and PPF-20

  • Added zinc nitrate hexahydrate, DPNI and TCPP to four vials.
    • insert chart with weights here
  • added 1.75 mL of leftover 75% DEF/25% EtOH to vials 1-3, 1 mL in vial 4
    • made a fresh solution of 75% DEF/25% EtOH and added 1mL to vial 4
    • added 250 μL of pure ethanol to vials 1-3
  • made a 10 mL solution of 1 M nitric acid in ethanol
    • 10 mL * 1 M = x mL * 15. 8M --> x= 1.58 mL conc nitric acid
    • --> added 1.58 mL of conc nitric acid to 8.46 mL of ethanol
  • added 100 μL of 1M HNO3 in EtOH to vials 1&2 and 80 μL to vials 3&4
  • sonciated vials and placed in oven at 3pm
    • programmed to heat at 80 °C for 24 hrs then cool to 0 °C (20 °Croom temp) over 9 hrs

Data/Spectra

  • Insert content here...

Notes

  • Insert content here...


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