User:Abigail E. Miller/Notebook/MOF Project/2013/01/25: Difference between revisions
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==Bench Work== | ==Bench Work== | ||
* | ====exchanging PPF-18 with guanine and adenine==== | ||
* | |||
====synthesizing PPF-18 and PPF-20==== | |||
* Added zinc nitrate hexahydrate, DPNI and TCPP to four vials. | |||
** insert chart with weights here | |||
*added 1.75 mL of leftover 75% DEF/25% EtOH to vials 1-3, 1 mL in vial 4 | |||
** made a fresh solution of 75% DEF/25% EtOH and added 1mL to vial 4 | |||
** added 250 μL of pure ethanol to vials 1-3 | |||
*made a 10 mL solution of 1 M nitric acid in ethanol | |||
** 10 mL * 1 M = x mL * 15. 8M --> x= 1.58 mL conc nitric acid | |||
** --> added 1.58 mL of conc nitric acid to 8.46 mL of ethanol | |||
* added 100 μL of 1M HNO3 in EtOH to vials 1&2 and 80 μL to vials 3&4 | |||
* sonciated vials and placed in oven at 3pm | |||
** programmed to heat at 80 °C for 24 hrs then cool to 0 °C (20 °Croom temp) over 9 hrs | |||
==Data/Spectra== | ==Data/Spectra== | ||
Revision as of 08:50, 29 January 2013
 Metal Organic Frameworks
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Objective
Bench Workexchanging PPF-18 with guanine and adeninesynthesizing PPF-18 and PPF-20
Data/Spectra
Notes
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