User:Abigail E. Miller/Notebook/MOF Project/2013/01/31: Difference between revisions
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==Bench Work== | ==Bench Work== | ||
* | * made a solution of 4, 4 bipyridine | ||
** 6 mg of 4, 4' bipyridine in 3 mL of DEF and 1 mL of ethanol | |||
* exchange the pillar from DPNI to 4, 4' bipyridine | |||
** 1:15 pm mixed 3 mL of hte above solution with 13 mg of PPF-18 | |||
** 4:30 pm filtered and dried the crystals | |||
*see Eleni's notebook for 3 vials of reactants for synthesizing PPF-18 | |||
** place the vials in the oven at 9am on 2/1/2013 to ehat for 24 hrs at 85 °C then cool to room temp over for 9 hrs. | |||
* react OD2A with zinc nitrate | |||
** see Matt's notebook for reactant amounts | |||
** heated for 2 hrs at 130 °C | |||
** let cool on bench top - some white crystals at hte bottom of hte vial | |||
**heated from 1-4:30pm at 130 °C | |||
** then turned off the oven and let it cool to room temp | |||
* | |||
==Data/Spectra== | ==Data/Spectra== | ||
Revision as of 15:59, 5 February 2013
 Metal Organic Frameworks
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Objective
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