User:Abigail E. Miller/Notebook/MOF Project/2013/02/05

From OpenWetWare

(Difference between revisions)
Jump to: navigation, search
Line 12: Line 12:
* need 500mg zinc nitrate hexahydrate (MW 297.5 g/mol), 154.3 mg Terephthalic acid (MW 166.13 g/mol) and either 63.5 mg guanine (MW 151.13 g/mol) or 56.8 mg adenine (MW 155.13 g/mol)
* need 500mg zinc nitrate hexahydrate (MW 297.5 g/mol), 154.3 mg Terephthalic acid (MW 166.13 g/mol) and either 63.5 mg guanine (MW 151.13 g/mol) or 56.8 mg adenine (MW 155.13 g/mol)
-
*  weighed out each component
+
*  weighed out each component into a vial.
-
** for IRMOF with guanine: 506.8 mg Zn(NO3)2 6H2O, 160 mg Terephthalic acid
+
** for IRMOF with guanine: 506.8 mg Zn(NO3)2 6H2O, 160 mg Terephthalic acid, 67 mg guanine
 +
** for IRMOF with adenine: 523.0 mg Zn(NO3)2 6H2O, 155 mg Terephthalic acid, 57.8 mg adenine
-
*  
+
* added approx 6 mL DMY to each vial
 +
 
 +
* sonicated to dissolve leaving IRMOF-G vial  with a white, opaque solution and the IFMOR-A vial with a clear transparent solution.
 +
 
 +
* at 4pm place at 90 °C in a oven.

Revision as of 17:31, 5 February 2013

Metal Organic Frameworks Main project page
Previous entry      

Objective

  • synthesis IRMOF's with adenine and guanine

Bench Work

  • need 500mg zinc nitrate hexahydrate (MW 297.5 g/mol), 154.3 mg Terephthalic acid (MW 166.13 g/mol) and either 63.5 mg guanine (MW 151.13 g/mol) or 56.8 mg adenine (MW 155.13 g/mol)
  • weighed out each component into a vial.
    • for IRMOF with guanine: 506.8 mg Zn(NO3)2 6H2O, 160 mg Terephthalic acid, 67 mg guanine
    • for IRMOF with adenine: 523.0 mg Zn(NO3)2 6H2O, 155 mg Terephthalic acid, 57.8 mg adenine
  • added approx 6 mL DMY to each vial
  • sonicated to dissolve leaving IRMOF-G vial with a white, opaque solution and the IFMOR-A vial with a clear transparent solution.
  • at 4pm place at 90 °C in a oven.


Data/Spectra

  • Insert content here...

Notes

  • Insert content here...


Personal tools