User:Abigail E. Miller/Notebook/MOF Project/2013/02/05
From OpenWetWare
(Difference between revisions)
| Line 12: | Line 12: | ||
* need 500mg zinc nitrate hexahydrate (MW 297.5 g/mol), 154.3 mg Terephthalic acid (MW 166.13 g/mol) and either 63.5 mg guanine (MW 151.13 g/mol) or 56.8 mg adenine (MW 155.13 g/mol) | * need 500mg zinc nitrate hexahydrate (MW 297.5 g/mol), 154.3 mg Terephthalic acid (MW 166.13 g/mol) and either 63.5 mg guanine (MW 151.13 g/mol) or 56.8 mg adenine (MW 155.13 g/mol) | ||
| - | * weighed out each component | + | * weighed out each component into a vial. |
| - | ** for IRMOF with guanine: 506.8 mg Zn(NO3)2 6H2O, 160 mg Terephthalic acid | + | ** for IRMOF with guanine: 506.8 mg Zn(NO3)2 6H2O, 160 mg Terephthalic acid, 67 mg guanine |
| + | ** for IRMOF with adenine: 523.0 mg Zn(NO3)2 6H2O, 155 mg Terephthalic acid, 57.8 mg adenine | ||
| - | * | + | * added approx 6 mL DMY to each vial |
| + | |||
| + | * sonicated to dissolve leaving IRMOF-G vial with a white, opaque solution and the IFMOR-A vial with a clear transparent solution. | ||
| + | |||
| + | * at 4pm place at 90 °C in a oven. | ||
Revision as of 18:31, 5 February 2013
Main project page Previous entry
| |
Objective
Bench Work
Data/Spectra
Notes
| |



