User:Alicia Rasines Mazo/Notebook/CHEM-581 Experimental Chemistry I/2014/09/26: Difference between revisions
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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span> | |style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span> | ||
|style="background-color: #F2F2F2" align="center"| | |style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]] }}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}} | ||
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==Tasks for September 26== | ==Tasks for September 26== | ||
* To | * To complete Wednesday's film synthesis | ||
* To begin new film synthesis | |||
===Completing film synthesis=== | |||
* Continued from [http://openwetware.org/index.php?title=User:Alicia_Rasines_Mazo/Notebook/CHEM-581_Experimental_Chemistry_I/2014/09/24&action=edit September 24] | |||
*Soaked in sodium sulfate for 1h, put into 0.1% HCl for 30 min, then sodium bicarbonate solution for a further 15 min. | |||
===Preparation of 10% wt new exfoliated clay films=== | |||
*1.0114 g 22,000 PVA, 0.1107 g of of exfoliated tributylhexadecylphosphonium bromide (THP Br) and 7 mL of distilled water were used to make up a 10% wt PVA-exfoliated THP Br film. Note this clay was prepared by Michael's group. | |||
*1.0290 g 22,000 PVA, 0.1105 g of exfoliated 1-hexadecyltriphenylphosphonium bromide and 7 mL of distilled water were used to make up a 10% wt PVA-exfoliated THP Br film. This clay was previously prepared by Eleni's group. | |||
*Heated at approx. 80ºC with gentle stirring until all crystals were dissolved | |||
*Allowed to cool down to room temeprature | |||
*Added 0.8 wt% 0.5 mL glutaraldehyde under hood | |||
*Stirred for 3 min to ensure homogeneity | |||
*Poured into teflon dish and allowed to dry | |||
Latest revision as of 00:21, 27 September 2017
Project name | Main project page Previous entry Next entry |
Tasks for September 26
Completing film synthesis
Preparation of 10% wt new exfoliated clay films
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