User:Allison K. Alix/Notebook/Thesis Research/2013/08/13: Difference between revisions

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==Entry title==
==Scaled up Silica-Coating Procedure==


    1mL AuNP & MHA solution/2μL TES/0.125mL NH4OH/5mL propanol  
Original: 1mL AuNP & MHA solution/2μL TES/0.125mL NH4OH/5mL propanol  


Re-scale to use 9mL AuNP/MHA solution
1) Re-scale to use 9mL AuNP/MHA solution
 
9mL AuNP&MHA solution/18uL TES/1.125mL NH4OH/45mL propanol


New: 9mL AuNP&MHA solution/18uL TES/1.125mL NH4OH/45mL propanol


2) Stir solutions for one hour to allow reaction to proceed
2) Stir solutions for one hour to allow reaction to proceed
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3) Centrifuge solutions at 4000 rpm for one hour
3) Centrifuge solutions at 4000 rpm for one hour


4) Re-suspend particles in water
4) Re-suspend particles in water  





Revision as of 08:22, 13 August 2013

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Scaled up Silica-Coating Procedure

Original: 1mL AuNP & MHA solution/2μL TES/0.125mL NH4OH/5mL propanol

1) Re-scale to use 9mL AuNP/MHA solution

New: 9mL AuNP&MHA solution/18uL TES/1.125mL NH4OH/45mL propanol

2) Stir solutions for one hour to allow reaction to proceed

3) Centrifuge solutions at 4000 rpm for one hour

4) Re-suspend particles in water