User:Andrew K Farag/Notebook/CHEM-571/2014/02/04: Difference between revisions
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Note: Much of the protocol for today will be determined by the results of our first synthesis. | Note: Much of the protocol for today will be determined by the results of our first synthesis. | ||
==Edited Protocol== | |||
* we are going to increase the final volume of solution to yield more mass to be collected. The original final volume will be multiplied by three. | |||
Corrected Volumes Table | |||
{| {{table}} | |||
| align="center" style="background:#f0f0f0;"|'''% BSA''' | |||
| align="center" style="background:#f0f0f0;"|'''5 mM Zinc Nitrate (uL)''' | |||
| align="center" style="background:#f0f0f0;"|'''5mM Manganese Acetate (uL)''' | |||
| align="center" style="background:#f0f0f0;"|'''41.65 mM Ammonium Acetate (uL)''' | |||
| align="center" style="background:#f0f0f0;"|'''11uM BSA* (uL)''' | |||
| align="center" style="background:#f0f0f0;"|'''10uM L-Cysteine (uL)''' | |||
| align="center" style="background:#f0f0f0;"|'''10mM Ammonium Hydroxide (uL)''' | |||
| align="center" style="background:#f0f0f0;"|'''5 mM Sodium Sulfide* (uL)''' | |||
| align="center" style="background:#f0f0f0;"|'''Total Volume (mL)''' | |||
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| 0||540||60||600||0||600||3000||600||5.4 | |||
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| 10||540||60||600||60||540||3000||600||5.4 | |||
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| 20||540||60||600||120||480||3000||600||5.4 | |||
|- | |||
| 30||540||60||600||180||420||3000||600||5.4 | |||
|- | |||
| 40||540||60||600||240||360||3000||600||5.4 | |||
|- | |||
| 50||540||60||600||300||300||3000||600||5.4 | |||
|- | |||
| 60||540||60||600||360||240||3000||600||5.4 | |||
|- | |||
| 70||540||60||600||420||180||3000||600||5.4 | |||
|- | |||
| 80||540||60||600||480||120||3000||600||5.4 | |||
|- | |||
| 90||540||60||600||540||60||3000||600||5.4 | |||
|- | |||
| 100||540||60||600||600||0||3000||600||5.4 | |||
|} | |||
==Data== | ==Data== |
Revision as of 10:25, 5 February 2014
Biomaterials Design Lab | <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page <html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html> </html>Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html> | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
ObjectiveCharacterize the previously synthesized BSA-L-cysteine ZnS:Mn Nanocrystals using UV-Vis. Protocol
Note: Much of the protocol for today will be determined by the results of our first synthesis. Edited Protocol
DataAll solutions in the test tube have orange fluorescence properties. All test tubes have precipitates, the largest with 0% BSA. UV-Vis and fluorescence measurements of all test tubes are recorded. NotesThis area is for any observations or conclusions that you would like to note.
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