User:Andrew K Farag/Notebook/CHEM-582/2015/01/30: Difference between revisions
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== | ==Objectives== | ||
#Find out the right proportions of materials used | |||
#Start one synthesis | |||
#Find the proper cross linking temperature | |||
==Materials== | |||
#DER 331, which is an undiluted diglycidyl ether of bisphenol A (DGEBA). | |||
#JEFFAMINE® D-400 amine | |||
#Titanium Dioxide T696 | |||
==Measurements== | |||
the proportion of Amine to Epoxy should be 1:1 in equivalent weights. | |||
The equivalent weight for the epoxy is 182-192 g/mol. | |||
The below image shows the equivalent weights of a few Jeffamines | |||
[[Image:Amine equivilent weights.PNG]] | |||
==Synthesis== | |||
#measure 3.0559 of JD-400 | |||
#add 5.5633 g of the epoxy | |||
#add 0.8473 g of TiO2 | |||
#let stir for 5 minutes with temperature of 85C | |||
#reduce the temperature to 50C for another 10 minutes. | |||
#transport the mixture into an aluminum dish | |||
#Let it sit in room temperature till next lab section. | |||
==DSC Test== | |||
#Weigh a pan and a lid | |||
#add the mixture in the pan and press the lid on it | |||
#Input into DSC to test for temperature starting at 20C to 200C, adding 5C/min | |||
##This test will let us know the optimum temperature for cross linking | |||
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Revision as of 13:16, 30 January 2015
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Objectives
Materials
Measurementsthe proportion of Amine to Epoxy should be 1:1 in equivalent weights. The equivalent weight for the epoxy is 182-192 g/mol. The below image shows the equivalent weights of a few Jeffamines Synthesis
DSC Test
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