User:Andrew K Farag/Notebook/CHEM-582/2015/02/04: Difference between revisions

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#add 5.53123 g of the epoxy
#add 5.53123 g of the epoxy
#let stir for 5 minutes with temperature of 85C
#let stir for 5 minutes with temperature of 85C
#reduce the temperature to 50C for another 10 minutes.
#reduce the temperature to 60C for another 10 minutes.
#transport the mixture into an aluminum dish  
#transport the mixture into an aluminum dish  
#Let it sit in room temperature till next lab section.
#Let it sit in room temperature till next lab section.

Revision as of 07:50, 4 February 2015

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Objectives

  1. Put the aluminum plate in the oven on temperature 85C for two hours
  2. Increase temperature to 135C for two more hours
  3. Repeat the synthesis from Friday, 30th of January, 2015
  4. Start a new synthesis, without the titatnium dioxide
  5. Analyze DSC Data

TiO2/Epoxy Film Synthesis

  1. measure 3.03450 g of JD-400
  2. add 5.52087 g of the epoxy
  3. add 0.84646 g of TiO2
  4. let stir for 5 minutes with temperature of 85C
  5. reduce the temperature to 60C for another 10 minutes.
  6. transport the mixture into an aluminum dish
  7. Let it sit in room temperature till next lab section.

Epoxy/No TiO2 present Synthesis

  1. measure 3.03840 g of JD-400
  2. add 5.53123 g of the epoxy
  3. let stir for 5 minutes with temperature of 85C
  4. reduce the temperature to 60C for another 10 minutes.
  5. transport the mixture into an aluminum dish
  6. Let it sit in room temperature till next lab section.



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