User:Dhea Patel/Notebook/Hemoglobin Project/2013/06/11

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The [http://openwetware.org/wiki/User:Paul_Rothenberg/Notebook/Pauls_Notebook/2013/05/31 procedure]for the reaction of OPD and H<sub>2</sub>O<sub>2</sub> was followed using a Mb/Tris catalyst and an acetonitrile suspension. Like [[User:Paul_Rothenberg/Notebook/Pauls_Notebook/2013/06/10| yesterday]], the reaction was run in a beaker with a stir bar and the solution was filtered before taking a spectrum.  
The [http://openwetware.org/wiki/User:Paul_Rothenberg/Notebook/Pauls_Notebook/2013/05/31 procedure]for the reaction of OPD and H<sub>2</sub>O<sub>2</sub> was followed using a Mb/Tris catalyst and an acetonitrile suspension. Like [[User:Paul_Rothenberg/Notebook/Pauls_Notebook/2013/06/10| yesterday]], the reaction was run in a beaker with a stir bar and the solution was filtered before taking a spectrum.  
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In addition reactions were run using Mb/Phosphate and Mb/Acetate in acetone suspension.
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In addition reactions were run using Mb/Phosphate and Mb/Acetate in acetone suspension.
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Because the acetone corroded the plastic, samples 80mins-140mins are taken without filtering the sample.
==Data==
==Data==
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<b>Mb/Phosphate in Acetone</b>
<b>Mb/Phosphate in Acetone</b>
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[[]]
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[[Image:Mb_Phosphate_OPD_H2O2_Acetone_WORKUP_GRAPH.png]]
<b>Mb/Acetate in Acetone</b>
<b>Mb/Acetate in Acetone</b>
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[[]]
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[[Image:Mb_Acetate_OPD_H2O2_Acetone_WORKUP_GRAPH.png]]
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Revision as of 16:08, 11 June 2013

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Reaction of OPD+H2O2 with Mb Catalyst in Acetonitrile Suspension

The procedurefor the reaction of OPD and H2O2 was followed using a Mb/Tris catalyst and an acetonitrile suspension. Like yesterday, the reaction was run in a beaker with a stir bar and the solution was filtered before taking a spectrum.

In addition reactions were run using Mb/Phosphate and Mb/Acetate in acetone suspension. Because the acetone corroded the plastic, samples 80mins-140mins are taken without filtering the sample.

Data

Mb/Tris in Acetonitrile

Image:Mb_Tris1_OPD_H2O2_MeCN_FILTERED_WORKUP_GRAPH.png

Note: The source was off during the 80mins measurement, so data was not available.

Image:Mb_Tris2_OPD_H2O2_MeCN_WORKUP_GRAPH.png


Mb/Phosphate in Acetone

Image:Mb_Phosphate_OPD_H2O2_Acetone_WORKUP_GRAPH.png

Mb/Acetate in Acetone

Image:Mb_Acetate_OPD_H2O2_Acetone_WORKUP_GRAPH.png


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