User:Dhea Patel/Notebook/Hemoglobin Project/2013/06/21: Difference between revisions

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==Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb Catalyst in Hexane Suspension==
==Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb Catalyst in Hexane Suspension==


The [http://openwetware.org/wiki/User:Paul_Rothenberg/Notebook/Pauls_Notebook/2013/05/31 procedure]for the reaction of OPD and H<sub>2</sub>O<sub>2</sub> was followed using a Mb/Acetate and Mb/Phosphate catalyst and a hexane suspension. The reaction was run in a beaker with a stir bar and the solution was filtered before taking a spectrum.
The [http://openwetware.org/wiki/User:Paul_Rothenberg/Notebook/Pauls_Notebook/2013/05/31 procedure]for the reaction of OPD and H<sub>2</sub>O<sub>2</sub> was followed using a Mb/Acetate and Mb/Phosphate catalyst and a hexane suspension. The OPD was sonicated for 30 minutes and the Mb was sonicated for 10 minutes. The reaction was run in a beaker with a stir bar and the solution was centrifuged before taking a spectrum.


==Data==
==Data==
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<b>Mb/Phosphate in Hexane, Trial 2</b>
<b>Mb/Phosphate in Hexane, Trial 2</b>


[[]]
[[Image:Mb_Phosphate_OPD_H2O2_Hexane_GRAPH_Trial2.png]]




<b>Mb/Acetate in Hexane, Trial 3</b>
<b>Mb/Acetate in Hexane, Trial 3</b>


[[]]
[[Image:Mb_Acetate_OPD_H2O2_Hexane_WORKUP_Trial3_GRAPH.JPG]]


<b>Mb/Phosphate in Hexane, Trial 3</b>
<b>Mb/Phosphate in Hexane, Trial 3</b>


[[]]
[[Image:Mb_Phosphate_OPD_H2O2_Hexane_WORKUP_Trial3_GRAPH.JPG]]





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Reaction of OPD+H2O2 with Mb Catalyst in Hexane Suspension

The procedurefor the reaction of OPD and H2O2 was followed using a Mb/Acetate and Mb/Phosphate catalyst and a hexane suspension. The OPD was sonicated for 30 minutes and the Mb was sonicated for 10 minutes. The reaction was run in a beaker with a stir bar and the solution was centrifuged before taking a spectrum.

Data

Mb/Acetate in Hexane, Trial 2

Mb/Phosphate in Hexane, Trial 2


Mb/Acetate in Hexane, Trial 3

Mb/Phosphate in Hexane, Trial 3