User:Dhea Patel/Notebook/Phosphorylation/2012/10/03

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Current revision (09:55, 3 October 2012) (view source)
(Description)
 
Line 17: Line 17:
--150mL acetonitrile + saturated sodium nitrate
--150mL acetonitrile + saturated sodium nitrate
 +
--100mL 90% acetonitrile + saturated sodium nitrate
--100mL 90% acetonitrile + saturated sodium nitrate
 +
--150mL 80% acetonitrile + saturated sodium nitrate
--150mL 80% acetonitrile + saturated sodium nitrate
 +
--400mL 70% acetonitrile + saturated sodium nitrate
--400mL 70% acetonitrile + saturated sodium nitrate
 +
--200mL 65% acetonitrile + saturated sodium nitrate
--200mL 65% acetonitrile + saturated sodium nitrate
 +
2 bands appeared. The second one was collected and rotovapped.
2 bands appeared. The second one was collected and rotovapped.

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Contents

Objective

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Description

  1. 0.22g Ru complex was purified in a silcia gel column, using a total of about 1.5L acetonitrile.

--150mL acetonitrile + saturated sodium nitrate

--100mL 90% acetonitrile + saturated sodium nitrate

--150mL 80% acetonitrile + saturated sodium nitrate

--400mL 70% acetonitrile + saturated sodium nitrate

--200mL 65% acetonitrile + saturated sodium nitrate


2 bands appeared. The second one was collected and rotovapped.

Data

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Notes

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