User:Dhea Patel/Notebook/Phosphorylation/2012/10/17: Difference between revisions

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==Objective==
==Objective==
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* to prepare and run RuATP column.


==Description==
==Description==
# Add experimental record here. Include what, how, and why...
*1.5L of 2:4:4:3 isopropanol:dioxane:water:25% ammonium hydride solution was made.  
*a [[User:Dhea_Patel/Notebook/Phosphorylation/2012/06/25| silica gel column]] was made to purify the RuATP. The isopropanol:dioxane:water:25% ammonium hydride was used as the solvent instead of acetonitrile. No variations in the solvent were used.
 
* purified Ru was dissolved in about 10mL of DMF before added to the ATP reaction.  


==Data==
==Data==

Revision as of 10:10, 17 October 2012

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Objective

  • to prepare and run RuATP column.

Description

  • 1.5L of 2:4:4:3 isopropanol:dioxane:water:25% ammonium hydride solution was made.
  • a silica gel column was made to purify the RuATP. The isopropanol:dioxane:water:25% ammonium hydride was used as the solvent instead of acetonitrile. No variations in the solvent were used.
  • purified Ru was dissolved in about 10mL of DMF before added to the ATP reaction.

Data

  • Add data and results here...

Notes

This area is for any observations or conclusions that you would like to note.