User:Elaine Marie Robbins/Notebook/CHEM-496/2011/10/19: Difference between revisions

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|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Synthesizing AuNP V</span>
|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> AuNP V</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
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==Objective==
==Objective==


To synthesize gold nanoparticles (Au NP) using the procedure developed here:  
To synthesize AuNPs using the procedure developed here:  




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==Description==
==Description==


# Combine 0.974 mL of 0.0154 mM BSA and 0.581 mL of 4.3 mM HAuCl<sub>4</sub> in a capped test tube at room temperature.
# Add water to a total volume of 10 mL
# Place reaction mixture in an oven at 80°C for 30 min under thermostatic conditions.
# Remove reaction mixture from oven and allow to sit at room temperature for 10 min.
# Repeat steps 3 and 4 for 3 hr.


==Data==
==Data==


 
Purple protein fibers appeared in solution.


==Notes==
==Notes==

Revision as of 10:00, 26 October 2011

AuNP V <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page
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Objective

To synthesize AuNPs using the procedure developed here:


Bakshi, Mandeep S.; Kaur, Harpreet; Khullar, Poonam, Banipal, Tarlok, S.; Kaur, Gurinder; Singh, Narpinder Journal of Physical Chemistry C 2011, 115(7), 2982-2992

http://pubs.acs.org/doi/abs/10.1021/jp110296y


In addition, to repeat the experiment performed on 08/31/11, 09/07/11, 09/27/11, and 09/28/11.

Description

  1. Combine 0.974 mL of 0.0154 mM BSA and 0.581 mL of 4.3 mM HAuCl4 in a capped test tube at room temperature.
  2. Add water to a total volume of 10 mL
  3. Place reaction mixture in an oven at 80°C for 30 min under thermostatic conditions.
  4. Remove reaction mixture from oven and allow to sit at room temperature for 10 min.
  5. Repeat steps 3 and 4 for 3 hr.

Data

Purple protein fibers appeared in solution.

Notes




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