User:Elaine Marie Robbins/Notebook/CHEM-496/2012/02/29: Difference between revisions

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|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Synthesizing AuNP Fibers</span>
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==Objective==
To make a solution of AuNP/BSA protein fibers and to continue to take UV-vis data over time of 70 Au/BSA solution synthesized on [[User:Elaine Marie Robbins/Notebook/CHEM-496/2012/01/31 |01/31/11]].
==Description==


# Make a solution with an Au/BSA mole ratio = 166
# Combine 1 mL of 3.66 mM HAuCl<sub>4</sub> and 1.27 mL of 0.0173 mM BSA in a test tube.
# Dilute to 10 mL with water.
# Place in oven at 80°C.
# Leave solutions in oven for 3.5 hr.
==Data==


* Synthesized protein fibers:


<center>[[Image:Fiber soltuion 2-29-12.JPG]]</center>


==Objective==
*Add your objective here
stuff [[User:Matt Hartings|Matt Hartings]] 21:41, 6 September 2011 (EDT)


==Description==
* 70 ratio AuNP solution, week 5:
*Add description here
more stuff [[User:Matt Hartings|Matt Hartings]] 21:43, 6 September 2011 (EDT)


==Data==
<center>[[Image:70 ratio AuNP soln week 5.JPG]]</center>
* Add data and results here...


==Notes==
The AuNP came out of solution. UV-vis data was taken of the clear solution. No absorbance was measured in the desired range.
This area is for any observations or conclusions that you would like to note.


<center>[[Image:Absorbance vs wavelength over time week 5.png]]</center>


Use categories like tags. Change the "Course" category to the one corresponding to your course. The "Miscellaneous" tag can be used for particular experiments, as instructed by your professor. Please be sure to change or delete this tag as required so that the categories remain well organized.
==Notes==


[[Category:Course]]
[[Category:Course]]
[[Category:Miscellaneous]]
[[Category:Miscellaneous]]




Revision as of 13:50, 29 February 2012

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Objective

To make a solution of AuNP/BSA protein fibers and to continue to take UV-vis data over time of 70 Au/BSA solution synthesized on 01/31/11.

Description

  1. Make a solution with an Au/BSA mole ratio = 166
  2. Combine 1 mL of 3.66 mM HAuCl4 and 1.27 mL of 0.0173 mM BSA in a test tube.
  3. Dilute to 10 mL with water.
  4. Place in oven at 80°C.
  5. Leave solutions in oven for 3.5 hr.

Data

  • Synthesized protein fibers:


  • 70 ratio AuNP solution, week 5:

The AuNP came out of solution. UV-vis data was taken of the clear solution. No absorbance was measured in the desired range.

Notes



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