Objective
- Finish the film synthesis from Friday, August 29
- Start a new film synthesis
- DSC analysis of soaked films
- FTIR analysis of soaked films
Protocol
- Finish the film synthesis
- follow the protocol from Friday August 29th
- Start new synthesis of Polymer and Polymer-clay films
- Using the synthesis method from Tuesday, August 26
- weigh pan and cap separately, record weight
- weigh out approximately 0.3mg of each film
- place then into a pan, and seal cap over each
- 10 samples total
- 4 polymer films that have been soaked in 2ppm, 8ppm, 80ppm, and 200ppm
- 4 polymer-clay films that have been soaked in 2ppm, 8ppm, 80ppm, and 200ppm
- 1 plane polymer film soaking in water, and 1 plane polymer-clay films soaking in water
- Input data information into the computer program (weights, position, reference)
- Place prepared capped trays into the machine and run analysis
- Tables of DSC preparation
Mass of Pan + Lid
|
Mass of PVA + Clay + MG
|
Concentration
|
0.05311 |
0.00312 |
2ppm
|
0.05234 |
0.00324 |
8ppm
|
0.05248 |
0.0042 |
80ppm
|
0.05213 |
0.00499 |
200ppm
|
Mass of Pan + Lid
|
Mass of PVA + MG
|
Concentration
|
0.05287 |
0.00385 |
2ppm
|
0.05269 |
0.00499 |
8ppm
|
0.05294 |
0.00316 |
80ppm
|
0.05285 |
0.00365 |
200pm
|
Mass of Pan + Lid
|
Mass of PVA
|
0.0527 |
0.00572
|
|
Mass of Pan + Lid
|
Mass of PVA + Clay
|
0.05248 |
0.0069
|
|
Data
Data
|