User:Eleni N. Kalivas/Notebook/CHEM-571/2014/09/12: Difference between revisions
From OpenWetWare
Line 14: | Line 14: | ||
==Protocol== | ==Protocol== | ||
====Exfoliated Clays==== | |||
Use 1.0045g of PVA in 2.7701g NaMT in order to make the 10% clay film. Using the same protocol as August 27th, 2014. | Use 1.0045g of PVA in 2.7701g NaMT in order to make the 10% clay film. Using the same protocol as August 27th, 2014. | ||
====Powder Xray diffraction==== | |||
Prepared a PVA-film soaked in 80ppm Malachite Green for XRD analysis. We secured the film to the holder using tape and an XRD of the tape alone has been taken for comparison. | Prepared a PVA-film soaked in 80ppm Malachite Green for XRD analysis. We secured the film to the holder using tape and an XRD of the tape alone has been taken for comparison. | ||
====Preparation of new Malachite Green (M.G.) solutions==== | |||
#200 ppm M.G. made by [[User:Madeleine Y. Bee/Notebook/CHEM-581 Experimental Chemistry/2014/09/12|Madeline Bee]] and calculations can be found on her page. | #200 ppm M.G. made by [[User:Madeleine Y. Bee/Notebook/CHEM-581 Experimental Chemistry/2014/09/12|Madeline Bee]] and calculations can be found on her page. | ||
#80ppm M.G. made using 40mL of the 200ppm in 100mL volumetric flask. | #80ppm M.G. made using 40mL of the 200ppm in 100mL volumetric flask. | ||
Line 26: | Line 26: | ||
#2ppm M.G. made by [[http://openwetware.org/wiki/User:James_C._Schwabacher/Notebook/CHEM-571/2014/09/12|James Schwabacher]] calculations can be found on his page. | #2ppm M.G. made by [[http://openwetware.org/wiki/User:James_C._Schwabacher/Notebook/CHEM-571/2014/09/12|James Schwabacher]] calculations can be found on his page. | ||
====Soaking PVA-Films in Malachite Green Solutions==== | |||
*200 ppm M.G. | *200 ppm M.G. | ||
**Vial mass: 13.1452 g | **Vial mass: 13.1452 g |
Revision as of 11:45, 12 September 2014
Project name | <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page <html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html> </html>Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html> |
Objective
ProtocolExfoliated ClaysUse 1.0045g of PVA in 2.7701g NaMT in order to make the 10% clay film. Using the same protocol as August 27th, 2014. Powder Xray diffractionPrepared a PVA-film soaked in 80ppm Malachite Green for XRD analysis. We secured the film to the holder using tape and an XRD of the tape alone has been taken for comparison. Preparation of new Malachite Green (M.G.) solutions
Soaking PVA-Films in Malachite Green Solutions
|