User:Ellen Petersen/Notebook/MOF/2012/04/12

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(DPNI Take 1)
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==DPNI Take 1==
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==DPNI: 04-12-12==
* 1.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol)
* 1.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol)
*2.) 4- aminopyridine (.847 g, 6.00 mmol)
*2.) 4- aminopyridine (.847 g, 6.00 mmol)

Revision as of 08:40, 25 June 2013

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DPNI: 04-12-12

  • 1.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol)
  • 2.) 4- aminopyridine (.847 g, 6.00 mmol)
  • 3.) Diethyl ether (600 mL
  • 4.) Dimethylacetamide (DMA) (150 mL)
  • Dissolve 1&2 in DMA stirred at 135 degrees C overnight.
  • Cooled to room temperature and poured onto diethyl ether (600 mL).
  • Precipitate filter and washed with diethyl ether
  • dried under vacuum to yield



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