User:Ellen Petersen/Notebook/MOF/2012/04/12

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Current revision (10:43, 28 June 2013) (view source)
 
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*4.) Dimethylacetamide (DMA) (150 mL)
*4.) Dimethylacetamide (DMA) (150 mL)
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*Dissolve 1&2 in DMA stirred at 135 degrees C overnight.
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*5.) Dissolve 1&2 in DMA stirred at 135 degrees C overnight.
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*Cooled to room temperature and poured onto diethyl ether (600 mL).
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*6.) Cooled to room temperature and poured onto diethyl ether (600 mL).
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*Precipitate filter and washed with diethyl ether
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*7.) Precipitate filter and washed with diethyl ether
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*dried under vacuum to yield  
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*8.) dried under vacuum to yield  

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DPNI: 04-12-12

  • 1.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol)
  • 2.) 4- aminopyridine (.847 g, 6.00 mmol)
  • 3.) Diethyl ether (600 mL
  • 4.) Dimethylacetamide (DMA) (150 mL)
  • 5.) Dissolve 1&2 in DMA stirred at 135 degrees C overnight.
  • 6.) Cooled to room temperature and poured onto diethyl ether (600 mL).
  • 7.) Precipitate filter and washed with diethyl ether
  • 8.) dried under vacuum to yield



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