User:Ellen Petersen/Notebook/MOF Continued/2013/02/22: Difference between revisions

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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> MOF: Tara </span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
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==Entry title==
==PPF-18==
==PPF-18==
* 1.) Add solids 5,10,15,20- Tetrakis(4-carboxyl)-21H,23H-porphine  (TCPP) (.0079 g, .01 mmol),Zinc nitrate hexahydrate (.0089  g, .03 mmol, N,N’-di-(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide (DPNI) (.0042 g, .01 mmol)to small capped vial
* 1.) Add solids 5,10,15,20- Tetrakis(4-carboxyl)-21H,23H-porphine  (TCPP) (.0079 g, .01 mmol),Zinc nitrate hexahydrate (.0089  g, .03 mmol, N,N’-di-(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide (DPNI) (.0042 g, .01 mmol)to small capped vial
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* 5.) Vacuum Filtration
* 5.) Vacuum Filtration
* 6.) Run Powder X-Ray Diffraction  
* 6.) Run Powder X-Ray Diffraction (See Image Below)
 
[[Image:022713.png‎|200px|Description of image]]
 




Revision as of 06:02, 28 June 2013

MOF: Tara <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page
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PPF-18

  • 1.) Add solids 5,10,15,20- Tetrakis(4-carboxyl)-21H,23H-porphine (TCPP) (.0079 g, .01 mmol),Zinc nitrate hexahydrate (.0089 g, .03 mmol, N,N’-di-(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide (DPNI) (.0042 g, .01 mmol)to small capped vial
  • 2.) Add 1.0 M nitric acid (50 μL, .05 mmol) in ethanol, N,N-diethyl formamide (DEF)(1.5 mL),Ethanol (0.5 mL)
  • 3.) Sealed and Sonicated to ensure homogeneity
  • 4.) Heated to 80° C in an oven for 24 hours followed by a slow cooling to room temperature for 9 hours

_____________________________________________________________________________________________________________________________________________ 02-23-2013

  • 5.) Vacuum Filtration
  • 6.) Run Powder X-Ray Diffraction (See Image Below)

Description of image



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