User:Ellen Petersen/Notebook/MOF Continued/2013/03/04

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==Entry title==
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==Filtering DPNI==
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* Insert content here...
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* 1.) Add 550 mL ethanol,
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* 2.) Vacuum Filtration to separate filter paper from DPNI solid
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_____________________________________________________________________________________________________________________________
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03-05-2013
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* 3.)Rotavap to separate solvent and solute, leftover is dark brown liquid
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* NMR: Liquid from Rotavap- Image 1
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* NMR: Solid from filtration- Figure 2
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Revision as of 10:50, 27 June 2013

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Filtering DPNI

  • 1.) Add 550 mL ethanol,
  • 2.) Vacuum Filtration to separate filter paper from DPNI solid

_____________________________________________________________________________________________________________________________ 03-05-2013

  • 3.)Rotavap to separate solvent and solute, leftover is dark brown liquid
  • NMR: Liquid from Rotavap- Image 1
  • NMR: Solid from filtration- Figure 2


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