User:Ellen Petersen/Notebook/MOF Continued/2013/03/06: Difference between revisions
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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> | |style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> MOF: Tara </span> | ||
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== | ==Remove amorphous material in PPF-18 & Synthesizing Sheets== | ||
* | |||
* 1.) Combine Vials ( EK 2/4/13, EMP 11/16/13, AEM 1/8/13, AEM 1/28/13) | |||
* 2.) Add .0092 g to small vial | |||
* 3.) Add 1.5 mL DEF, .5 mL ethanol, .0175014 g Adenine | |||
*Powder X-Ray Diffraction taken of PPF-18, and PPF-18 with adenine | |||
[[Image:31313.png|200px|PPF-18]] | |||
[[Image:031313.png|200px|PPF-18 with Adenine]] | |||
[[Image:032713.png|200px|PPF-18 with Adenine]] | |||
_________________________________________________________________________________________________________________ | |||
03-06-13 | |||
*Synthesizing Sheets: | |||
*1.) Add 7.9 mg (0.01 mmol) TCPP, 8.9 (0.03 mmmol) zinc nitrate, 1.5 mL DEF, .5 mL ethanol, 1.0 M nitric acid (50 μL, .05 mmol) in ethanol | |||
*2.) Sonification | |||
*3.) Heat 24 hours, cool down 9 hours | |||
03-19-13 | |||
*4.) Filtration | |||
03-20-13 | |||
*5.) Powder X-Ray Diffraction (See Image 1 below) | |||
[[Image:032012.png|200px|Sheets]] | |||
Revision as of 06:26, 28 June 2013
MOF: Tara | <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page <html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html> </html>Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html> |
Remove amorphous material in PPF-18 & Synthesizing Sheets
_________________________________________________________________________________________________________________ 03-06-13
03-19-13
03-20-13
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