User:Ellen Petersen/Notebook/MOF Continued/2013/03/19: Difference between revisions
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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> | |style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> MOF: Tara </span> | ||
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== | ==PPF-18== | ||
* | * 1.) Add solids 5,10,15,20- Tetrakis(4-carboxyl)-21H,23H-porphine (TCPP) (.0079 g, .01 mmol),Zinc nitrate hexahydrate (.0089 g, .03 mmol, N,N’-di-(4-pyridyl)-1,4,5,8-naphthalenetetracarboxydiimide (DPNI) (.0042 g, .01 mmol)to small capped vial | ||
* 2.) Add 1.0 M nitric acid (50 μL, .05 mmol) in ethanol, N,N-diethyl formamide (DEF)(1.5 mL),Ethanol (0.5 mL) | |||
* 3.) Sealed and Sonicated to ensure homogeneity | |||
* 4.) Heated to 80° C in an oven for 24 hours followed by a slow cooling to room temperature for 9 hours (Program 2) | |||
_____________________________________________________________________________________________________________________________________________ | |||
03-20-2013 | |||
* 5.) Vacuum Filtration | |||
* 6.) Run Powder X- Diffraction | |||
_______________________________________________________________________________________________________________________________________________ | |||
03-22-2013 | |||
*7.) Soack in 2 mL DMF | |||
*8.) Vacuum Filtration | |||
Revision as of 09:20, 27 June 2013
MOF: Tara | <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page <html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html> </html>Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html> |
PPF-18
_____________________________________________________________________________________________________________________________________________ 03-20-2013
_______________________________________________________________________________________________________________________________________________ 03-22-2013
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