User:Ellen Petersen/Notebook/Metal Organic Frameworks/Entry Base: Difference between revisions
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== | ==DPNI: 04-12-12== | ||
1.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol) | |||
2.) 4- aminopyridine (.847 g, 6.00 mmol) | |||
3.) Diethyl ether (600 mL | |||
4.) Dimethylacetamide (DMA) (150 mL) | |||
5.) Dissolve 1&2 in DMA stirred at 135 degrees C overnight. | |||
6.) Cooled to room temperature and poured onto diethyl ether (600 mL). | |||
7.) Precipitate filter and washed with diethyl ether | |||
8.) dried under vacuum to yield | |||
Revision as of 06:08, 25 June 2013
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<html><img src="/images/9/94/Report.png" border="0" /></html> Main project page |
DPNI: 04-12-121.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol) 2.) 4- aminopyridine (.847 g, 6.00 mmol) 3.) Diethyl ether (600 mL 4.) Dimethylacetamide (DMA) (150 mL) 5.) Dissolve 1&2 in DMA stirred at 135 degrees C overnight. 6.) Cooled to room temperature and poured onto diethyl ether (600 mL). 7.) Precipitate filter and washed with diethyl ether 8.) dried under vacuum to yield
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