User:Helen L. Slucher/Notebook/CHEM-572/2014/01/28: Difference between revisions

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# 1.158mL of 10mM HAuCl4 added to 50mL of water
# 1.158mL of 10mM HAuCl4 added to 50mL of water
# Heat solution until it boils
# 0.5mL of 10mg/mL citrate sodium added to solution and heated until color changes from dark blue to red
* Making HAuCl4
* Making HAuCl4
**Add 0.0413g HAuCl3 to 10mL volumetric flask
**Add 0.0413g HAuCl3 to 10mL volumetric flask
*Made Sodium citrate solution
*Making sodium citrate solution
**Add 0.250g sodium citrate into 25mL volumetric flask
**Add 0.250g sodium citrate into 25mL volumetric flask
# Heat solution until it boils
<br>
# 0.5mL of 10mg/mL citrate sodium added to solution and heated until color changes from dark blue to red
 
Determine the size of the nanoparticle solution
Determine the size of the nanoparticle solution


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**Possible that not enough gold was added
**Possible that not enough gold was added
*We then made a new solution where we added 2mLs of 10.48mM gold solution
*We then made a new solution where we added 2mLs of 10.48mM gold solution
**The solution turned blue and then red after the sodium citrate was added
==UV/Vis==
[[Image:Screen Shot 2014-01-28 at 2.57.00 PM.png]]
# Random
# Correct
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Revision as of 12:57, 28 January 2014

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Procedure

Make citrate gold nanoparticles

  1. 1.158mL of 10mM HAuCl4 added to 50mL of water
  2. Heat solution until it boils
  3. 0.5mL of 10mg/mL citrate sodium added to solution and heated until color changes from dark blue to red
  • Making HAuCl4
    • Add 0.0413g HAuCl3 to 10mL volumetric flask
  • Making sodium citrate solution
    • Add 0.250g sodium citrate into 25mL volumetric flask


Determine the size of the nanoparticle solution

Data

  • We heated the above solution and it did not turn blue
    • Possible that not enough gold was added
  • We then made a new solution where we added 2mLs of 10.48mM gold solution
    • The solution turned blue and then red after the sodium citrate was added

UV/Vis

  1. Random
  2. Correct