User:Jacob Esenther/Notebook/581/2014/09/05: Difference between revisions
From OpenWetWare
No edit summary |
No edit summary |
||
Line 18: | Line 18: | ||
# Finish the synthesis of clay films started on 09/03. The procedure may be viewed [[User:Jacob_Esenther/Notebook/581/2014/08/29|here]]. | # Finish the synthesis of clay films started on 09/03. The procedure may be viewed [[User:Jacob_Esenther/Notebook/581/2014/08/29|here]]. | ||
# FTIR | # Fourier Transform Infrared Spectroscopy (FTIR) | ||
## We will be using attenuated total reflectance ([http://en.wikipedia.org/wiki/Attenuated_total_reflectance ATR]) mode for our samples | ## We will be using attenuated total reflectance ([http://en.wikipedia.org/wiki/Attenuated_total_reflectance ATR]) mode for our samples | ||
## Place the film in the sample holder. Execute measurement | ## Place the film in the sample holder. Execute measurement | ||
Line 29: | Line 29: | ||
## Wait for all measurements to be taken | ## Wait for all measurements to be taken | ||
==Data== | ==New Film Data== | ||
Film Synthesis | Film Synthesis | ||
* 0.9997g PVA | * 0.9997g PVA | ||
* 1.0142g PVA +0.1038g Cloisite | * 1.0142g PVA +0.1038g Cloisite | ||
DSC Prep | ==DSC Prep Data== | ||
[[Image:DSC_Pan_measurements.jpg]] | [[Image:DSC_Pan_measurements.jpg]] | ||
==FTIR of MG Sample Film Data | |||
[[Image:PVA FTIR MJJ 09052014 revised.png|800x580px|center|thumb|Polyvinyl Alcohol Films with Absorbed Malachite Green Concentrations; 0.2, 0.5, 1.1, 1.4, 1.7, and 2.0 ppm]] | |||
[[Image:PVA clay FTIR MJJ 09052014 revised.png|800x579px|center|thumb|Polyvinyl Alcohol and Sodium Montmorillonite Films with Absorbed Malachite Green Concentrations; 0.2, 0.5, 1.1, 1.4, 1.7, and 2.0 ppm]] | |||
==Notes== | ==Notes== |
Revision as of 07:30, 24 September 2014
Biomaterials Design Lab | <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page <html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html> </html>Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html> |
Objective
Description
New Film DataFilm Synthesis
DSC Prep Data==FTIR of MG Sample Film Data NotesWhen handling the pans in preparation for the DSC, two different sets of forceps should be used. One for handling the films and one for handling the pan. The reason being that water on the outside of the pan will skew measurements. This is a visual of the different films and their absorbance of the Malachite Green.
|