User:James C. Schwabacher/Notebook/Protein-Templated Quantum Dots/2014/09/16: Difference between revisions

From OpenWetWare
Jump to navigationJump to search
(fix raw html notebook nav)
 
(One intermediate revision by one other user not shown)
Line 2: Line 2:
|-
|-
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
|style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}}
|-
|-
| colspan="2"|
| colspan="2"|
Line 8: Line 8:
==Objective==
==Objective==
* Synthesize HgS-BSA QDs at 40°C |'''JCS 2'''
* Synthesize HgS-BSA QDs at 40°C |'''JCS 2'''
* Obtain UVVis and fluorescence data
* Obtain UVVis and fluorescence data for JCS 1


==Protocol==
==Protocol==

Latest revision as of 00:17, 27 September 2017

Project name Main project page
Previous entry      Next entry

Objective

  • Synthesize HgS-BSA QDs at 40°C |JCS 2
  • Obtain UVVis and fluorescence data for JCS 1

Protocol

  1. Making Stock Solutions
    1. Same stock solutions from last week
  2. Synthesis
    1. Added 5 mL of 15mg/mL BSA from Eleni's stock solution to 5 mL of the HgNO3 in HPLC water
    2. stirred vigorously while adding 2 drops of 1 M NaOH to reach pH ~9
    3. capped to sit and react for ~12 hours

Notes

  • The HgNO3 solution was sonicated for 15 minutes prior to use.
  • The pH test trip was slightly darker than the coding for a pH 9 (~pH 10), like the last synthesis. This time only 50 μL of 1M NaOH was added.
  • The heating mantle was set to 11. As of this afternoon, this corresponded to about 41°C



Retrieved from "https://openwetware.org/mediawiki/index.php?title=User:James_C._Schwabacher/Notebook/Protein-Templated_Quantum_Dots/2014/09/16&oldid=1015318"