User:James C. Schwabacher/Notebook/Protein-Templated Quantum Dots/2015/02/27: Difference between revisions
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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Protein-Templated Quantum Dots</span> | |style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Protein-Templated Quantum Dots</span> | ||
|style="background-color: #F2F2F2" align="center"| | |style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]] }}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}} | ||
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* While I previously reported preparing a DSC sample with one of the later reactions (I recorded the pan mass, etc.), this sample was never run. The instrument was not working at the time and the sample sat for too long by the time the DSC was up and running. | * While I previously reported preparing a DSC sample with one of the later reactions (I recorded the pan mass, etc.), this sample was never run. The instrument was not working at the time and the sample sat for too long by the time the DSC was up and running. | ||
* A collection of images taken throughout the year have been labeled and uploaded to DropBox as well. | * A collection of images taken throughout the year have been labeled and uploaded to DropBox as well. | ||
*Note: Un-rotovapped samples that were left sitting in the scintillation vials in the cold room formed a layer of precipitate on the bottom of the glass. The best way to describe these structures is 'shiny aluminum foil.' | |||
==Original Protocol== | ==Original Protocol== |
Latest revision as of 00:55, 27 September 2017
Protein-Templated Quantum Dots | Main project page Previous entry | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Project Summary
Original Protocol
"Quick" Protocol (15 min Synthesis)
Note: These solutions have a tendency to bump on the rotovap. Watch carefully and be ready to break vacuum temporarily in the beginning!Filtration ProtocolI conducted vacuum filtration once using a membrane filter (Supor-450, 47mm, 0.45μm). This worked to separate the gels from the solution, however do not leave the product on the membrane to dry--it will get stuck the membrane. Summary of Syntheses Attempted
Determining Sol-Gel formation factors
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