User:James C. Schwabacher/Notebook/Protein-Templated Quantum Dots/2015/02/27: Difference between revisions
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* You will find UV-Vis and Fluorescence data for the first few syntheses (JCS 1-3) in an excel file on DropBox. This file also contains FTIR data from JCS 16. The sample was stuck to the membrane that was used to filter it, so a spectra of the membrane is also included. | * You will find UV-Vis and Fluorescence data for the first few syntheses (JCS 1-3) in an excel file on DropBox. This file also contains FTIR data from JCS 16. The sample was stuck to the membrane that was used to filter it, so a spectra of the membrane is also included. | ||
* There is a folder containing the DSC data for films JCS 4 and JCS 5 on DropBox. | * There is a folder containing the DSC data for films JCS 4 and JCS 5 on DropBox. | ||
* You will also find a folder containing powder XRD data for the films produced from JCS 4 and JCS 5. | * You will also find a folder containing powder XRD data for the films produced from JCS 4 and JCS 5. However, something went wrong with the DSC protocol during the runs so these results should be scrutinized. | ||
* While I previously reported preparing a DSC sample with one of the later reactions (I recorded the pan mass, etc.), this sample was never run. The instrument was not working at the time and the sample sat for too long by the time the DSC was up and running. | |||
* A collection of images taken throughout the year have been labeled and uploaded to DropBox as well. | * A collection of images taken throughout the year have been labeled and uploaded to DropBox as well. | ||
Revision as of 12:22, 23 April 2015
Protein-Templated Quantum Dots | <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page <html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html> </html> | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Project Summary
Original Protocol
"Quick" Protocol (15 min Synthesis)
Note: These solutions have a tendency to bump on the rotovap. Watch carefully and be ready to break vacuum temporarily in the beginning!Filtration ProtocolI conducted vacuum filtration once using a membrane filter (Supor-450, 47mm, 0.45μm). This worked to separate the gels from the solution, however do not leave the product on the membrane to dry--it will get stuck the membrane. Summary of Syntheses Attempted
Determining Sol-Gel formation factors
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