User:Jamie Nunziata/Notebook/Biomaterial Design 2016/2016/04/12: Difference between revisions

From OpenWetWare
Jump to navigationJump to search
(fix raw html notebook nav)
 
(One intermediate revision by one other user not shown)
Line 2: Line 2:
|-
|-
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
|style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}}
|-
|-
| colspan="2"|
| colspan="2"|
Line 21: Line 21:


==Data==
==Data==
Figure 1: FTIR of functionalized Gold Nanoparticles
<b>Figure 1:</b> FTIR of functionalized Gold Nanoparticles
<br>[[Image:JMB FTIRanalysis phytoremediation 571.png]]
<br>[[Image:JMB FTIRanalysis phytoremediation 571.png]]


Latest revision as of 01:44, 27 September 2017

Project name Main project page
Previous entry      Next entry

Objective

Today's objective includes the following:

  1. To prepare KBr Pellets for analysis of our capped nanoparticles using FT-IR.
  2. To prepare samples for analysis using ICP

Protocol

FTIR potassium bromide pellets were made using the following procedure:
250 mg of KBr was dissolved in approximately 25mL of 11-mercaptoundacanamide, 11-mercapto-1-undecanol, lysozyme, and citrate gold nanoparticles. The samples were frozen with liquid nitrogen and lyophilized for two days. The samples were then pelleted and analyzed using Bruker Alpha FT-IR Spectrometer.

ICP was performed using the following:
Standards of gold, sulfur, and the ions in the spring water were made in order to run ICP. 1, 5, 10, 20, and 30 ppm ICP ion standard solution was diluted with 3.0 M nitric acid (HNO3). 1, 7, 14, 21, 28, and 35 ppm gold standard solutions and sulfur standard solutions were diluted with HNO3. Each standard was 30 mL. Standards are run on the ICP first, in order to create a calibration curve. 25% dilution samples at of 15 mL before and after plant absorption are run.



Data

Figure 1: FTIR of functionalized Gold Nanoparticles



Retrieved from "https://openwetware.org/mediawiki/index.php?title=User:Jamie_Nunziata/Notebook/Biomaterial_Design_2016/2016/04/12&oldid=1018221"