User:Karlena L. Brown/Notebook/PVOH Research/2012/10/19: Difference between revisions
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==Crosslinking Porphyrin Films== | ==Crosslinking Porphyrin Films== | ||
'''Follow same | '''Follow same protocol regarding crosslinking glutaldehyde films 9/25/12; however, pay attention to the two PVOH films that will not be placed in the fixant solution during the crosslinking procedure.''' | ||
{| {{table}} | |||
| align="center" style="background:#f0f0f0;"|'''Films Prepared''' | |||
| align="center" style="background:#f0f0f0;"|'''PVOH 22K Amount (g)''' | |||
| align="center" style="background:#f0f0f0;"|'''Glutaldehyde Amount (mL)''' | |||
| align="center" style="background:#f0f0f0;"|'''Porphyrin Amount (mL)''' | |||
| align="center" style="background:#f0f0f0;"|'''HCl Addition (Y/N)''' | |||
|- | |||
| PVOH 22K w/ GA & PP(g)||1.0073||1.0||1.0||N | |||
|- | |||
| PVOH 22K w/ GA & PP(g)||1.0067||1.0||1.0||Y | |||
|- | |||
| PVOH 22K w/ GA & PP(g)||1.0523||0.5||1.0||N | |||
|- | |||
| PVOH 22K w/ GA & PP(g)||1.0211||0.5||1.0||Y | |||
|} | |||
==Notes== | ==Notes== |
Revision as of 21:28, 23 November 2012
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OBJECTIVES
New CuSO4 Dilution Standards for Atomic Absorption
(20 ppm CuSO4)V1 = (0.1 ppm CuSO4)(12mL) V1 = 0.6mL of 20 ppm CuSO4
(20 ppm CuSO4)V1 = (0.5 ppm CuSO4)(12mL) V1 = 1.2mL of 20 ppm CuSO4
(20 ppm CuSO4)V1 = (1 ppm CuSO4)(12mL) V1 = 3mL of 20 ppm CuSO4
(20 ppm CuSO4)V1 = (2 ppm CuSO4)(12mL) V1 = 6mL of 20 ppm CuSO4
(20 ppm CuSO4)V1 = (3 ppm CuSO4)(12mL) V1 = 9mL of 20 ppm CuSO4 Using the following concentrations(shown above), a calibration curve was prepared.
Atomic Absorption NaMT-CuSO4 Exchanged Filtrate Solutions
Fixant Solution Preparation
(Actual Na2SO4 Mass: 199.9953g)
Crosslinking Porphyrin FilmsFollow same protocol regarding crosslinking glutaldehyde films 9/25/12; however, pay attention to the two PVOH films that will not be placed in the fixant solution during the crosslinking procedure.
Notes |