User:Karlena L. Brown/Notebook/PVOH Research/2012/10/31: Difference between revisions
From OpenWetWare
(→Notes) |
|||
(5 intermediate revisions by the same user not shown) | |||
Line 28: | Line 28: | ||
==Films Examined using FTIR== | ==Films Examined using FTIR== | ||
'''RECALL FTIR PROCEDURAL PROTOCOL 9/17/12''' | '''RECALL FTIR PROCEDURAL PROTOCOL 9/17/12''' | ||
'''LIST OF FILMS FOR FTIR:''' | |||
#PVOH(22K) 1.0067g+1mL GA+1mL porphyrin crosslinked | |||
#PVOH(22K)+0.5mL GA+0.104g NaMT crosslinked spun 10 min CuSO4 prepared 10/17/2012 | |||
#PVOH(22K)+0.5mLGA+0.99mL porphyrin(no color on film )crosslinked prepared 10/19/2012 | |||
#PVOH(22K)+1mL GA+100%CEC crosslinked prepared 10/4/2012 | |||
#PVOH(22K)+1mL GA+1mL porphyrin crosslinked prepared 10/24/2012 | |||
#PVOH(22K)+0.5mL GA+1mL porphyrin crosslinked prepared 10/24/2012 #2 | |||
#PVOH(22K)+0.5mLGA+1mL porphyrin prepared crosslinked 10/26/2012 | |||
#PVOH(22K)+0.8wt% GA+100%CEC crosslinked spun 10 min CuSO4 prepared 10/26/2012 | |||
#PVOH(22K)+0.8wt% GA+50% CEC crosslinked spun 10 min CuSO4 prepared 10/17/2012 | |||
[[Image:FTIR.JPG]] | |||
==Ion Diffusion & Ion Selective Electrode Film Procedures== | ==Ion Diffusion & Ion Selective Electrode Film Procedures== | ||
Line 46: | Line 59: | ||
'''Ensure the hole separating the two graduated cylinder columns is completely shielded and covered by the PVOH 22K film''' | '''Ensure the hole separating the two graduated cylinder columns is completely shielded and covered by the PVOH 22K film''' | ||
== | ==Ion Diffusion Film Analysis: Varied Ion Solution== | ||
'''A crosslinked PVOH 22K film containing 1mL glutaldehyde that had been exchanged for 10 min in the CuSO<sub>4</sub> solution was used for an Ion Selective Electrode Analysis.''' | '''A crosslinked PVOH 22K film containing 1mL glutaldehyde that had been exchanged for 10 min in the CuSO<sub>4</sub> solution was used for an Ion Selective Electrode Analysis.''' | ||
Line 76: | Line 89: | ||
|} | |} | ||
== | ==Ion Diffusion Film Analysis: HPLC Grade H<sub>2</sub>O Solution== | ||
'''A crosslinked PVOH 22K film containing 1mL glutaldehyde that had been exchanged for 10 min in the CuSO<sub>4</sub> solution was used for an Ion Selective Electrode Analysis.''' | '''A crosslinked PVOH 22K film containing 1mL glutaldehyde that had been exchanged for 10 min in the CuSO<sub>4</sub> solution was used for an Ion Selective Electrode Analysis.''' | ||
Revision as of 11:49, 30 November 2012
PVOH Research | <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page <html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html> </html>Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html> | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
OBJECTIVES
Furfural Film Preparation
(PVOH 22K Actual Mass = 1.0029g)
(Furfural Actual Mass = 0.3192g)
Films Examined using FTIRRECALL FTIR PROCEDURAL PROTOCOL 9/17/12 LIST OF FILMS FOR FTIR:
Ion Diffusion & Ion Selective Electrode Film Procedures
Ensure the hole separating the two graduated cylinder columns is completely shielded and covered by the PVOH 22K film Ion Diffusion Film Analysis: Varied Ion SolutionA crosslinked PVOH 22K film containing 1mL glutaldehyde that had been exchanged for 10 min in the CuSO4 solution was used for an Ion Selective Electrode Analysis.
Ion Diffusion Film Analysis: HPLC Grade H2O SolutionA crosslinked PVOH 22K film containing 1mL glutaldehyde that had been exchanged for 10 min in the CuSO4 solution was used for an Ion Selective Electrode Analysis.
Notes
|