User:Karlena L. Brown/Notebook/PVOH Research/2012/10/31 - Revision history

Karlena L. Brown: /* Films Examined using FTIR */

2012-12-15T04:49:55Z

Films Examined using FTIR

←Older revision		Revision as of 04:49, 15 December 2012
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	'''LIST OF FILMS FOR FTIR:'''		'''LIST OF FILMS FOR FTIR:'''
-	#PVOH(22K) 1.0067g+1mL GA+1mL porphyrin crosslinked	+	{\| {{table}}
-	#PVOH(22K)+0.5mL GA+0.104g NaMT crosslinked spun 10 min CuSO4 prepared 10/17/2012	+	\| align="center" style="background:#f0f0f0;"\|'''Films'''
-	#PVOH(22K)+0.5mLGA+0.99mL porphyrin(no color on film )crosslinked prepared 10/19/2012	+	\| align="center" style="background:#f0f0f0;"\|'''New mass(g)'''
-	#PVOH(22K)+1mL GA+100%CEC crosslinked prepared 10/4/2012	+	\|-
-	#PVOH(22K)+1mL GA+1mL porphyrin crosslinked prepared 10/24/2012	+	\| PVOH(22K) 1.0067g+1mL GA+1mL porphyrin crosslinked\|\|1.7688
-	#PVOH(22K)+0.5mL GA+1mL porphyrin crosslinked prepared 10/24/2012 #2	+	\|-
-	#PVOH(22K)+0.5mLGA+1mL porphyrin prepared crosslinked 10/26/2012	+	\| PVOH(22K)+0.5mL GA+0.104g NaMT crosslinked spun 10 min CuSO4 prepared 10/17/2012\|\|0.9465
-	#PVOH(22K)+0.8wt% GA+100%CEC crosslinked spun 10 min CuSO4 prepared 10/26/2012	+	\|-
-	#PVOH(22K)+0.8wt% GA+50% CEC crosslinked spun 10 min CuSO4 prepared 10/17/2012	+	\| PVOH(22K)+0.5mLGA+0.99mL porphyrin(no color on film )crosslinked prepared 10/19/2012\|\|1.8045
-		+	\|-
		+	\| PVOH(22K)+1mL GA+100%CEC crosslinked prepared 10/4/2012\|\|1.3662
		+	\|-
		+	\| PVOH(22K)+1mL GA+1mL porphyrin crosslinked prepared 10/24/2012\|\|1.5477
		+	\|-
		+	\| PVOH(22K)+0.5mL GA+1mL porphyrin crosslinked prepared 10/24/2012 #2\|\|1.9685
		+	\|-
		+	\| PVOH(22K)+0.5mLGA+1mL porphyrin prepared crosslinked 10/26/2012\|\|2.1206
		+	\|-
		+	\| PVOH(22K)+0.8wt% GA+100%CEC crosslinked spun 10 min CuSO4 prepared 10/26/2012\|\|1.24
		+	\|-
		+	\| PVOH(22K)+0.8wt% GA+50% CEC crosslinked spun 10 min CuSO4 prepared 10/17/2012\|\|1.074
		+	\|}
		+	<br>
	[[Image:FTIR.JPG]]		[[Image:FTIR.JPG]]

Karlena L. Brown: /* Films Examined using FTIR */

2012-11-30T18:49:22Z

Films Examined using FTIR

←Older revision		Revision as of 18:49, 30 November 2012
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	'''RECALL FTIR PROCEDURAL PROTOCOL 9/17/12'''		'''RECALL FTIR PROCEDURAL PROTOCOL 9/17/12'''

-	LIST OF FILMS FOR FTIR:	+	'''LIST OF FILMS FOR FTIR:'''
	#PVOH(22K) 1.0067g+1mL GA+1mL porphyrin crosslinked		#PVOH(22K) 1.0067g+1mL GA+1mL porphyrin crosslinked
	#PVOH(22K)+0.5mL GA+0.104g NaMT crosslinked spun 10 min CuSO4 prepared 10/17/2012		#PVOH(22K)+0.5mL GA+0.104g NaMT crosslinked spun 10 min CuSO4 prepared 10/17/2012

Karlena L. Brown: /* Films Examined using FTIR */

2012-11-30T18:46:44Z

Films Examined using FTIR

←Older revision		Revision as of 18:46, 30 November 2012
Line 28:		Line 28:
	==Films Examined using FTIR==		==Films Examined using FTIR==
	'''RECALL FTIR PROCEDURAL PROTOCOL 9/17/12'''		'''RECALL FTIR PROCEDURAL PROTOCOL 9/17/12'''
		+
		+	LIST OF FILMS FOR FTIR:
		+	#PVOH(22K) 1.0067g+1mL GA+1mL porphyrin crosslinked
		+	#PVOH(22K)+0.5mL GA+0.104g NaMT crosslinked spun 10 min CuSO4 prepared 10/17/2012
		+	#PVOH(22K)+0.5mLGA+0.99mL porphyrin(no color on film )crosslinked prepared 10/19/2012
		+	#PVOH(22K)+1mL GA+100%CEC crosslinked prepared 10/4/2012
		+	#PVOH(22K)+1mL GA+1mL porphyrin crosslinked prepared 10/24/2012
		+	#PVOH(22K)+0.5mL GA+1mL porphyrin crosslinked prepared 10/24/2012 #2
		+	#PVOH(22K)+0.5mLGA+1mL porphyrin prepared crosslinked 10/26/2012
		+	#PVOH(22K)+0.8wt% GA+100%CEC crosslinked spun 10 min CuSO4 prepared 10/26/2012
		+	#PVOH(22K)+0.8wt% GA+50% CEC crosslinked spun 10 min CuSO4 prepared 10/17/2012
		+
	[[Image:FTIR.JPG]]		[[Image:FTIR.JPG]]

Karlena L. Brown: /* Films Examined using FTIR */

2012-11-30T18:08:34Z

Films Examined using FTIR

←Older revision		Revision as of 18:08, 30 November 2012
Line 29:		Line 29:
	'''RECALL FTIR PROCEDURAL PROTOCOL 9/17/12'''		'''RECALL FTIR PROCEDURAL PROTOCOL 9/17/12'''
	[[Image:FTIR.JPG]]		[[Image:FTIR.JPG]]
-	br

	==Ion Diffusion & Ion Selective Electrode Film Procedures==		==Ion Diffusion & Ion Selective Electrode Film Procedures==

Karlena L. Brown: /* Films Examined using FTIR */

2012-11-30T18:08:21Z

Films Examined using FTIR

←Older revision		Revision as of 18:08, 30 November 2012
Line 28:		Line 28:
	==Films Examined using FTIR==		==Films Examined using FTIR==
	'''RECALL FTIR PROCEDURAL PROTOCOL 9/17/12'''		'''RECALL FTIR PROCEDURAL PROTOCOL 9/17/12'''
		+	[[Image:FTIR.JPG]]
		+	br

	==Ion Diffusion & Ion Selective Electrode Film Procedures==		==Ion Diffusion & Ion Selective Electrode Film Procedures==

Karlena L. Brown: /* ISE Film Analysis: HPLC Grade H2O Solution */

2012-11-24T09:48:15Z

ISE Film Analysis: HPLC Grade H2O Solution

←Older revision		Revision as of 09:48, 24 November 2012
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	\|}		\|}

-	==~~ISE~~ Film Analysis: HPLC Grade H<sub>2</sub>O Solution==	+	==Ion Diffusion Film Analysis: HPLC Grade H<sub>2</sub>O Solution==
	'''A crosslinked PVOH 22K film containing 1mL glutaldehyde that had been exchanged for 10 min in the CuSO<sub>4</sub> solution was used for an Ion Selective Electrode Analysis.'''		'''A crosslinked PVOH 22K film containing 1mL glutaldehyde that had been exchanged for 10 min in the CuSO<sub>4</sub> solution was used for an Ion Selective Electrode Analysis.'''

Karlena L. Brown: /* ISE Film Analysis: Varied Ion Solution */

2012-11-24T09:47:58Z

ISE Film Analysis: Varied Ion Solution

←Older revision		Revision as of 09:47, 24 November 2012
Line 46:		Line 46:
	'''Ensure the hole separating the two graduated cylinder columns is completely shielded and covered by the PVOH 22K film'''		'''Ensure the hole separating the two graduated cylinder columns is completely shielded and covered by the PVOH 22K film'''

-	==~~ISE~~ Film Analysis: Varied Ion Solution==	+	==Ion Diffusion Film Analysis: Varied Ion Solution==
	'''A crosslinked PVOH 22K film containing 1mL glutaldehyde that had been exchanged for 10 min in the CuSO<sub>4</sub> solution was used for an Ion Selective Electrode Analysis.'''		'''A crosslinked PVOH 22K film containing 1mL glutaldehyde that had been exchanged for 10 min in the CuSO<sub>4</sub> solution was used for an Ion Selective Electrode Analysis.'''

Karlena L. Brown: /* Notes */

2012-11-24T09:47:04Z

Notes

←Older revision		Revision as of 09:47, 24 November 2012
Line 108:		Line 108:
	==Notes==		==Notes==
	* The varied ion concentrated solution contained the following ions: Chlorine (Cl<sup>-</sup>), Bromine (Br<sup>-</sup>), and Iodine (I<sup>-</sup>).		* The varied ion concentrated solution contained the following ions: Chlorine (Cl<sup>-</sup>), Bromine (Br<sup>-</sup>), and Iodine (I<sup>-</sup>).
-	* μS/cm (~~microsemen~~ per centimeter) is a conductivity unit of measurement that is the inverse of an Ohm (O).	+	* μS/cm (microsiemen per centimeter) is a conductivity unit of measurement that is the inverse of an Ohm (O).
	* Experimental readings regarding the Ion Selective Electrode Analysis were taken every 30 minutes; however, for the first reading and recording only a 10 min interval surpassed before a reading was taken.		* Experimental readings regarding the Ion Selective Electrode Analysis were taken every 30 minutes; however, for the first reading and recording only a 10 min interval surpassed before a reading was taken.
	* The final two readings germane to the Ion Selective Electrode Analysis for the PVOH 22K film containing 1mL glutaldehyde that was exchanged for 10 min with CuSO<sub>4</sub> were taken by Dr. Fox.		* The final two readings germane to the Ion Selective Electrode Analysis for the PVOH 22K film containing 1mL glutaldehyde that was exchanged for 10 min with CuSO<sub>4</sub> were taken by Dr. Fox.

Karlena L. Brown: /* Ion Diffusion & Ion Selective Electrode Film Procedures */

2012-11-24T09:46:41Z

Ion Diffusion & Ion Selective Electrode Film Procedures

←Older revision		Revision as of 09:46, 24 November 2012
Line 36:		Line 36:
	# Then, in other graduated cylinder column pour in ~20mL of the varied ion concentrated solution		# Then, in other graduated cylinder column pour in ~20mL of the varied ion concentrated solution
	# Plug the electrodes into the SympHony meter and turn on the ion selective electrode instruments		# Plug the electrodes into the SympHony meter and turn on the ion selective electrode instruments
-	# Then press the arrows until ISE (ion selective electrode) and μS/cm (~~microsemen~~ per centimeter) appear on the screen	+	# Then press the arrows until ISE (ion selective electrode) and μS/cm (microsiemen per centimeter) appear on the screen
	# Remove the electrodes from the storage solutions		# Remove the electrodes from the storage solutions
	# Rinse the electrodes with distilled H<sub>2</sub>O and thoroughly dry both with KimWipes		# Rinse the electrodes with distilled H<sub>2</sub>O and thoroughly dry both with KimWipes

Karlena L. Brown: /* Ion Diffusion & Ion Selective Electrode Film Procedures */

2012-11-24T09:45:21Z

Ion Diffusion & Ion Selective Electrode Film Procedures

←Older revision		Revision as of 09:45, 24 November 2012
Line 32:		Line 32:
	# Cut small piece of PVOH 22K film containing 1mL glutaldehyde exchanged in CuSO<sub>4</sub> for 10 min		# Cut small piece of PVOH 22K film containing 1mL glutaldehyde exchanged in CuSO<sub>4</sub> for 10 min
	# Place small cut piece of PVOH 22K film in plastic double graduated cylinder apparatus		# Place small cut piece of PVOH 22K film in plastic double graduated cylinder apparatus
-	~~'''Ensure the hole separating the two graduated cylinder columns is completely shielded and covered by the PVOH 22K film'''~~
	# Close and seal plastic double graduated cylinder apparatus		# Close and seal plastic double graduated cylinder apparatus
	# Next, in one graduated cylinder column pour in ~ 20mL of HPLC Grade H<sub>2</sub>O		# Next, in one graduated cylinder column pour in ~ 20mL of HPLC Grade H<sub>2</sub>O
Line 40:		Line 39:
	# Remove the electrodes from the storage solutions		# Remove the electrodes from the storage solutions
	# Rinse the electrodes with distilled H<sub>2</sub>O and thoroughly dry both with KimWipes		# Rinse the electrodes with distilled H<sub>2</sub>O and thoroughly dry both with KimWipes
-	# Place each electrode directly into the graduated cylinder columns containing either the HPLC Grade H<sub>2</sub>O or the varied ion solution for analysis (one electrode per column)	+	# Place each electrode directly into the graduated cylinder columns containing either the HPLC Grade H<sub>2</sub>O or the varied ion solution for analysis (one electrode per graduated column)
	# Measure the total amount of solution available and present for each graduated cylinder column		# Measure the total amount of solution available and present for each graduated cylinder column
	# Let each solution and electrode equilibrate for a set period of time (between 2-5 minutes) and then press measure on each instrument		# Let each solution and electrode equilibrate for a set period of time (between 2-5 minutes) and then press measure on each instrument
	# Once the measurement is finalized, record the values observed for each solution		# Once the measurement is finalized, record the values observed for each solution
		+
		+	'''Ensure the hole separating the two graduated cylinder columns is completely shielded and covered by the PVOH 22K film'''

	==ISE Film Analysis: Varied Ion Solution==		==ISE Film Analysis: Varied Ion Solution==