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PVOH Research
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OBJECTIVES
- Continue to clean, filter, and separate out the oil from the previously prepared microspheres on 2/22/13
- Prepare more microsphere samples expanding upon new previous method developed (new modifications)
PVOH 146K & 130K Prepared Microsphere Samples & Dye Preparations 4
RECALL MICROSPHERE PREPARATION PROTOCOL ON 2/20/13
1μM Rhodamine 6G Dye Concentration (90:10)
M1V1 = M2V2
1μM (RG6)x 10mL = (92μM)V2 V2 = 109μL
1μM Rhodamine 6G Dye Concentration (50:50)
M1V1 = M2V2
1μM (RG6)x 10mL = (165μM)V2 V2 = 61μL
PVOH vs. Clay Ratio
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Clay Selection
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PVOH 146K Mass (g)
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Actual Clay Mass (g)
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H2O Added (mL)
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Dye Concentration (μM)
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Dye Amount Added (μL)
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50:50 |
110% CEC NaMT w/ DMHXLBR |
0.05010 |
0.05100 |
40 |
165 |
61
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90:10 |
110% CEC NaMT w/ DMHXLBR |
0.01070 |
0.09100 |
40 |
92 |
109
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PVOH vs. Clay Ratio
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Clay Selection
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PVOH 130K Mass (g)
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Actual Clay Mass (g)
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H2O Added (mL)
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Dye Concentration (μM)
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Dye Amount Added (μL)
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50:50 |
110% CEC NaMT w/ DMHXLBR |
0.05070 |
0.05130 |
40 |
165 |
61
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90:10 |
110% CEC NaMT w/ DMHXLBR |
0.01090 |
0.09340 |
40 |
92 |
109
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