User:Karlena L. Brown/Notebook/PVOH Research/2013/03/20: Difference between revisions

From OpenWetWare
Jump to navigationJump to search
Line 10: Line 10:
* Prepare more microsphere samples expanding upon new previous method developed (new modifications)
* Prepare more microsphere samples expanding upon new previous method developed (new modifications)


==PVOH 146K & 130K Prepared Microsphere Samples & Dye Preparations 4==
==PVOH 146K Prepared Microsphere Samples & Dye Preparations 4==
'''RECALL MICROSPHERE PREPARATION PROTOCOL ON 2/20/13'''
'''RECALL MICROSPHERE PREPARATION PROTOCOL ON 2/20/13'''


Line 34: Line 34:
| 90:10||110% CEC NaMT w/ DMHXLBR||0.01070||0.09100||40||92||109
| 90:10||110% CEC NaMT w/ DMHXLBR||0.01070||0.09100||40||92||109
|}
|}
==PVOH 130K Prepared Microsphere Samples & Dye Preparations==
'''RECALL MICROSPHERE PREPARATION PROTOCOL ON 2/20/13'''
'''1μM Rhodamine 6G Dye Concentration (90:10)'''
  M<sub>1</sub>V<sub>1</sub> = M<sub>2</sub>V<sub>2</sub>
  1μM (RG6)x 10mL = (92μM)V<sub>2</sub>    V<sub>2</sub> = 109μL
'''1μM Rhodamine 6G Dye Concentration (50:50)'''
  M<sub>1</sub>V<sub>1</sub> = M<sub>2</sub>V<sub>2</sub>
  1μM (RG6)x 10mL = (165μM)V<sub>2</sub>    V<sub>2</sub> = 61μL


{| {{table}}
{| {{table}}

Revision as of 13:19, 24 March 2013

PVOH Research <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page
<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>

OBJECTIVES

  • Continue to clean, filter, and separate out the oil from the previously prepared microspheres on 2/22/13
  • Prepare more microsphere samples expanding upon new previous method developed (new modifications)

PVOH 146K Prepared Microsphere Samples & Dye Preparations 4

RECALL MICROSPHERE PREPARATION PROTOCOL ON 2/20/13

1μM Rhodamine 6G Dye Concentration (90:10) 

  M1V1 = M2V2
  1μM (RG6)x 10mL = (92μM)V2    V2 = 109μL

1μM Rhodamine 6G Dye Concentration (50:50) 

  M1V1 = M2V2
  1μM (RG6)x 10mL = (165μM)V2    V2 = 61μL
PVOH vs. Clay Ratio Clay Selection PVOH 146K Mass (g) Actual Clay Mass (g) H2O Added (mL) Dye Concentration (μM) Dye Amount Added (μL)
50:50 110% CEC NaMT w/ DMHXLBR 0.05010 0.05100 40 165 61
90:10 110% CEC NaMT w/ DMHXLBR 0.01070 0.09100 40 92 109

PVOH 130K Prepared Microsphere Samples & Dye Preparations

RECALL MICROSPHERE PREPARATION PROTOCOL ON 2/20/13

1μM Rhodamine 6G Dye Concentration (90:10) 

  M1V1 = M2V2
  1μM (RG6)x 10mL = (92μM)V2    V2 = 109μL

1μM Rhodamine 6G Dye Concentration (50:50) 

  M1V1 = M2V2
  1μM (RG6)x 10mL = (165μM)V2    V2 = 61μL
PVOH vs. Clay Ratio Clay Selection PVOH 130K Mass (g) Actual Clay Mass (g) H2O Added (mL) Dye Concentration (μM) Dye Amount Added (μL)
50:50 110% CEC NaMT w/ DMHXLBR 0.05070 0.05130 40 165 61
90:10 110% CEC NaMT w/ DMHXLBR 0.01090 0.09340 40 92 109

Notes

  • Unfortunately, DSC samples were not taken before the Rhodamine 6G dye was added; therefore, these samples must be remade.


Retrieved from "https://openwetware.org/mediawiki/index.php?title=User:Karlena_L._Brown/Notebook/PVOH_Research/2013/03/20&oldid=685245"