User:Karlena L. Brown/Notebook/PVOH Research/2013/03/20

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(PVOH 146K & 130K Prepared Microsphere Samples & Dye Preparations 4)
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==Notes==
==Notes==
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* Unfortunately, DSC samples were not taken before the Rhodamine 6G dye was added; therefore, these samples must be remade again.
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* Unfortunately, DSC samples were not taken before the Rhodamine 6G dye was added; therefore, these samples must be remade.
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Revision as of 15:13, 24 March 2013

PVOH Research Main project page
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OBJECTIVES

  • Continue to clean, filter, and separate out the oil from the previously prepared microspheres on 2/22/13
  • Prepare more microsphere samples expanding upon new previous method developed (new modifications)

PVOH 146K & 130K Prepared Microsphere Samples & Dye Preparations 4

RECALL MICROSPHERE PREPARATION PROTOCOL ON 2/20/13

1μM Rhodamine 6G Dye Concentration (90:10)

  M1V1 = M2V2
  1μM (RG6)x 10mL = (92μM)V2    V2 = 109μL

1μM Rhodamine 6G Dye Concentration (50:50)

  M1V1 = M2V2
  1μM (RG6)x 10mL = (165μM)V2    V2 = 61μL
PVOH vs. Clay Ratio Clay Selection PVOH 146K Mass (g) Actual Clay Mass (g) H2O Added (mL) Dye Concentration (μM) Dye Amount Added (μL)
50:50110% CEC NaMT w/ DMHXLBR0.050100.051004016561
90:10110% CEC NaMT w/ DMHXLBR0.010700.091004092109
PVOH vs. Clay Ratio Clay Selection PVOH 130K Mass (g) Actual Clay Mass (g) H2O Added (mL) Dye Concentration (μM) Dye Amount Added (μL)
50:50110% CEC NaMT w/ DMHXLBR0.050700.051304016561
90:10110% CEC NaMT w/ DMHXLBR0.010900.093404092109

Notes

  • Unfortunately, DSC samples were not taken before the Rhodamine 6G dye was added; therefore, these samples must be remade.


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