User:Karlena L. Brown/Notebook/PVOH Research/2013/03/22: Difference between revisions

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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> PVOH Research</span>
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> PVOH Research</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
|style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}}
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| align="center" style="background:#f0f0f0;"|'''Actual Clay Mass (g)'''
| align="center" style="background:#f0f0f0;"|'''Actual Clay Mass (g)'''
| align="center" style="background:#f0f0f0;"|'''H<sub>2</sub>O Added (mL)'''
| align="center" style="background:#f0f0f0;"|'''H<sub>2</sub>O Added (mL)'''
| align="center" style="background:#f0f0f0;"|'''Dye Concentration (μM)'''
| align="center" style="background:#f0f0f0;"|'''Safflower Oil Added (mL)'''
| align="center" style="background:#f0f0f0;"|'''Dye Amount Added (μL)'''
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| 50:50||NaMT||0.02530||0.02530||40||165||61
| 50:50||NaMT||0.02530||0.02530||20||35
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| 50:50||Laponite||0.02590||0.02500||40||165||61
| 50:50||Laponite||0.02590||0.02500||20||35
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| 90:10||NaMT||0.04140||0.01110||40||92||109
| 90:10||NaMT||0.04140||0.01110||20||35
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| 90:10||Laponite||0.04470||0.01100||40||92||109
| 90:10||Laponite||0.04470||0.01100||20||35
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| 50:50||110% CEC Laponite w/ DMHXLBR||0.02550||0.02500||40||165||61
| 50:50||110% CEC Laponite w/ DMHXLBR||0.02550||0.02500||20||35
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| 90:10||110% CEC Laponite w/ DMHXLBR||0.04230||0.01150||40||92||109
| 90:10||110% CEC Laponite w/ DMHXLBR||0.04230||0.01150||20||35
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| 50:50||50% CEC NaMT w/ Bu<sub>3</sub>HdP<sup>+</sup>||0.02540||0.02500||40||165||61
| 50:50||50% CEC NaMT w/ Bu<sub>3</sub>HdP<sup>+</sup>||0.02540||0.02500||20||35
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| 90:10||50% CEC NaMT w/ Bu<sub>3</sub>HdP<sup>+</sup>||0.04010||0.01050||40||92||109
| 90:10||50% CEC NaMT w/ Bu<sub>3</sub>HdP<sup>+</sup>||0.04010||0.01050||20||35
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Latest revision as of 22:34, 26 September 2017

PVOH Research Main project page
Previous entry      Next entry

OBJECTIVES

  • Prepare more microsphere samples expanding upon new previous method developed (new modifications)

PVOH 130K Prepared Microsphere Samples & Dye Preparations 2

RECALL MICROSPHERE PREPARATION PROTOCOL ON 2/20/13

1μM Rhodamine 6G Dye Concentration (90:10) 

  M1V1 = M2V2
  1μM (RG6)x 10mL = (92μM)V2    V2 = 109μL

1μM Rhodamine 6G Dye Concentration (50:50) 

  M1V1 = M2V2
  1μM (RG6)x 10mL = (165μM)V2    V2 = 61μL
PVOH vs. Clay Ratio Clay Selection PVOH 146K Mass (g) Actual Clay Mass (g) H2O Added (mL) Safflower Oil Added (mL)
50:50 NaMT 0.02530 0.02530 20 35
50:50 Laponite 0.02590 0.02500 20 35
90:10 NaMT 0.04140 0.01110 20 35
90:10 Laponite 0.04470 0.01100 20 35
50:50 110% CEC Laponite w/ DMHXLBR 0.02550 0.02500 20 35
90:10 110% CEC Laponite w/ DMHXLBR 0.04230 0.01150 20 35
50:50 50% CEC NaMT w/ Bu3HdP+ 0.02540 0.02500 20 35
90:10 50% CEC NaMT w/ Bu3HdP+ 0.04010 0.01050 20 35

Notes

  • Originally, samples were being prepared on a 0.1 gram scale; however, since then samples were divided into 1/4. New modifications include:
  # 50:50 clay vs. PVOH samples, the max amount being used is 0.025 grams for each substance
  # 90:10 clay vs. PVOH samples, the max amount being used is 0.01 grams clay and 0.04 grams PVOH
  • Based upon new sample modifications using 1/4 the original ratio, microsphere samples have began to form actual smaller microspheres rather than microgels or connected large clumps of spheres
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