User:Karlena L. Brown/Notebook/PVOH Research/2013/04/03: Difference between revisions
(fix raw html notebook nav) |
|||
(14 intermediate revisions by one other user not shown) | |||
Line 2: | Line 2: | ||
|- | |- | ||
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> PVOH Research</span> | |style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> PVOH Research</span> | ||
|style="background-color: #F2F2F2" align="center"| | |style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]] }}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}} | ||
|- | |- | ||
| colspan="2"| | | colspan="2"| | ||
Line 8: | Line 8: | ||
==OBJECTIVES== | ==OBJECTIVES== | ||
* Collect all DSC results from dry clay samples previously prepared on '''2/08/13''' | * Collect all DSC results from dry clay samples previously prepared on '''2/08/13''' | ||
* Run DSC sample analysis on | * Run DSC sample analysis on microsphere samples previously prepared on '''3/29/13''' | ||
* Remove all excess oil from controlled microsphere samples prepared on '''03/29/13''' | * Remove all excess oil from controlled microsphere samples prepared on '''03/29/13''' | ||
* Run fluorescence analysis on all microsphere samples prepared '''02/20/13''' with Rhodamine 6G dye | * Run fluorescence analysis on all microsphere samples prepared '''02/20/13''' with Rhodamine 6G dye | ||
==DSC Results for Dry Clay Samples== | ==DSC Results for Dry Clay Samples== | ||
[[Image:50% CEC NAMT.jpg]] | [[Image:50% CEC NAMT.jpg|400px]] | ||
[[Image:110 LP DMHXLBR.png|500px]] | |||
[[Image:110 NaMT DMHXLBR.png|500px]] | |||
[[Image:Laponite.png|500px]] | |||
[[Image:NaMT.png|500px]] | |||
[[Image:90-10 146K LP.png|500px]] | |||
==DSC Analysis: Mixed Microspheres== | ==DSC Analysis: Mixed Microspheres== | ||
Line 64: | Line 69: | ||
Figure 1 - Microsphere 90:10 PVOH 146K 50% CEC NaMT w/ Bu<sub>3</sub>HdP<sup>+</sup> | Figure 1 - Microsphere 90:10 PVOH 146K 50% CEC NaMT w/ Bu<sub>3</sub>HdP<sup>+</sup> | ||
<br> | <br> | ||
[[Image:90 pva 146 50NaMT micros diffusion.jpg]] | [[Image:90 pva 146 50NaMT micros diffusion.jpg|400px]] | ||
<br> | <br> | ||
''***Fluorescence intensity maximum is 6.985'' | ''***Fluorescence intensity maximum is 6.985'' | ||
Line 71: | Line 76: | ||
Figure 2 - Microsphere 90:10 PVOH 146K 110% CEC Laponite w/ DMHXLBR | Figure 2 - Microsphere 90:10 PVOH 146K 110% CEC Laponite w/ DMHXLBR | ||
<br> | <br> | ||
[[Image:90 PVA 146 110LP micros diff.jpg]] | [[Image:90 PVA 146 110LP micros diff.jpg|400px]] | ||
<br> | <br> | ||
''***Fluorescence intensity maximum is 5.109'' | ''***Fluorescence intensity maximum is 5.109'' | ||
Line 78: | Line 83: | ||
Figure 3 - Microsphere 90:10 PVOH 146K NaMT | Figure 3 - Microsphere 90:10 PVOH 146K NaMT | ||
<br> | <br> | ||
[[Image:90 PVA 146 NaMT micros diff test.png]] | [[Image:90 PVA 146 NaMT micros diff test.png|400px]] | ||
<br> | <br> | ||
''***Fluorescence intensity maximum is 26.734'' | ''***Fluorescence intensity maximum is 26.734'' | ||
Line 85: | Line 90: | ||
Figure 4 - Microsphere 50:50 PVOH 146K NaMT | Figure 4 - Microsphere 50:50 PVOH 146K NaMT | ||
<br> | <br> | ||
[[Image:50 PVA 146 NaMT micros diff.png]] | [[Image:50 PVA 146 NaMT micros diff.png|400px]] | ||
''***Fluorescence intensity maximum is 17.'' | ''***Fluorescence intensity maximum is 17.'' | ||
Line 91: | Line 96: | ||
Figure 5 - Microsphere 50:50 PVOH 146K 50% CEC NaMT w/ Bu<sub>3</sub>HdP<sup>+</sup> | Figure 5 - Microsphere 50:50 PVOH 146K 50% CEC NaMT w/ Bu<sub>3</sub>HdP<sup>+</sup> | ||
<br> | <br> | ||
[[Image:50 PVA 146 50NaMT micros diff.png]] | [[Image:50 PVA 146 50NaMT micros diff.png|400px]] | ||
<br> | <br> | ||
''***Fluorescence intensity maximum is 11.661'' | ''***Fluorescence intensity maximum is 11.661'' | ||
Line 98: | Line 103: | ||
Figure 6 - Microsphere 50:50 PVOH 146K 110% CEC Laponite w/ DMHXLBR | Figure 6 - Microsphere 50:50 PVOH 146K 110% CEC Laponite w/ DMHXLBR | ||
<br> | <br> | ||
[[Image:50 PVA 146 110 LP.png]] | [[Image:50 PVA 146 110 LP.png|400px]] | ||
<br> | <br> | ||
''***Fluorescence intensity maximum is 137.319'' | ''***Fluorescence intensity maximum is 137.319'' |
Latest revision as of 22:37, 26 September 2017
PVOH Research | Main project page Previous entry Next entry | |||||||||||||||||||||
OBJECTIVES
DSC Results for Dry Clay SamplesDSC Analysis: Mixed MicrospheresDSC preparation and protocol involving instrumentation and usage can be found on 9/17/12 entry.
# Equilibrate sample at ~ -40°C # Ramp sample temperature up from 20-240°C # Ramp sample temperature down from 20-(-40°C) # Repeat segment #2 again Fluorescence Analysis: Diffusion Testing 2RECALL DIFFUSION TESTING PROTOCOL ON 2/15/13
# Microsphere 90:10 PVOH 146K 50% CEC NaMT w/ Bu3HdP+ # Microsphere 90:10 PVOH 146K 110% CEC Laponite w/ DMHXLBR # Microsphere 90:10 PVOH 146K NaMT # Microsphere 50:50 PVOH 146K NaMT # Microsphere 50:50 PVOH 146K 50% CEC NaMT w/ Bu3HdP+ # Microsphere 50:50 PVOH 146K 110% CEC Laponite w/ DMHXLBR
# Excitation: 480nm # Emission Range: 500-650nm # Excitation Slit Width: 10 # Emission Slit Width: 10 # Scan Speed: 1200 Fluorescence Results & Spectrums
Notes
|