User:Karlena L. Brown/Notebook/PVOH Research/2013/04/03: Difference between revisions
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* Run DSC sample analysis on dry clay samples previously prepared on '''3/29/13''' | * Run DSC sample analysis on dry clay samples previously prepared on '''3/29/13''' | ||
* Remove all excess oil from controlled microsphere samples prepared on '''03/29/13''' | * Remove all excess oil from controlled microsphere samples prepared on '''03/29/13''' | ||
* Run fluorescence analysis on all microsphere samples prepared '''02/20/13''' with Rhodamine 6G dye | * Run fluorescence analysis on all microsphere samples prepared '''02/20/13''' with Rhodamine 6G dye | ||
==DSC Results for Dry Clay Samples== | ==DSC Results for Dry Clay Samples== |
Revision as of 22:00, 14 April 2013
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OBJECTIVES
DSC Results for Dry Clay SamplesDSC Analysis: Mixed MicrospheresDSC preparation and protocol involving instrumentation and usage can be found on 9/17/12 entry.
# Equilibrate sample at ~ -40°C # Ramp sample temperature up from 20-240°C # Ramp sample temperature down from 20-(-40°C) # Repeat segment #2 again Fluorescence Analysis: Diffusion Testing 2RECALL DIFFUSION TESTING PROTOCOL ON 2/15/13
# Microsphere 90:10 PVOH 146K 50% CEC NaMT w/ Bu3HdP+ # Microsphere 90:10 PVOH 146K 110% CEC Laponite w/ DMHXLBR # Microsphere 90:10 PVOH 146K NaMT # Microsphere 50:50 PVOH 146K NaMT # Microsphere 50:50 PVOH 146K 50% CEC NaMT w/ Bu3HdP+ # Microsphere 50:50 PVOH 146K 110% CEC Laponite w/ DMHXLBR
# Excitation: 480nm # Emission Range: 500-650nm # Excitation Slit Width: 10 # Emission Slit Width: 10 # Scan Speed: 1200 Fluorescence Results & Spectrums
Notes
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