User:Madeleine Y. Bee/Notebook/CHEM-581 Experimental Chemistry/2014/08/29: Difference between revisions

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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:20px;"> Film Syntheses, Make Stock Solutions</span>
|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> CHEM 581: Experimental Chemistry</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
|style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}}
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===Procedures===
===Procedures===
====Completing Film Synthesis====
====Completing Film Synthesis====
Continued from [http://openwetware.org/wiki/User:Madeleine_Y._Bee/Notebook/CHEM-581_Experimental_Chemistry/2014/08/27 Wednesday, 8/27/2014]
Continued from [http://openwetware.org/wiki/User:Madeleine_Y._Bee/Notebook/CHEM-581_Experimental_Chemistry/2014/08/27 Wednesday, 8/27/2014]<br.>
Procedure detailed by [http://openwetware.org/wiki/User:Matt_Hartings/Notebook/AU_Biomaterials_Design_Lab/2014/08/29 Dr Hartings]
*Stir in Sodium Sulfate, 1% HCl, and Sodium Bicarbonate solutions
*Stir in Sodium Sulfate, 1% HCl, and Sodium Bicarbonate solutions


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Procedure detailed by [http://openwetware.org/index.php?title=User:Matt_Hartings/Notebook/AU_Biomaterials_Design_Lab/2014/08/26&action=edit Dr Hartings]
Procedure detailed by [http://openwetware.org/index.php?title=User:Matt_Hartings/Notebook/AU_Biomaterials_Design_Lab/2014/08/26&action=edit Dr Hartings]
*Polymer-10% Clay Film
*Polymer-10% Clay Film
**1.0050g PVA and 0.12g sodium montmorillonite (~1g PVA and ~.1g NaM)
**1.0039g PVA and 0.1128g sodium montmorillonite (~1g PVA and ~.1g NaM)
*Polymer Film
*Polymer Film
**1.0036g PVA (~1g)
**1.0036g PVA (~1g)
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**(1.7ppm)(25mL)=(8.0ppm)*V
**(1.7ppm)(25mL)=(8.0ppm)*V
**V=5.31mL of 8.0ppm solution in 19.69mL water
**V=5.31mL of 8.0ppm solution in 19.69mL water
Take UV-vis measurements
====Soaking Films in Malachite Green Solutions====
*Polymer Film in 10 mL 2 ppm Malachite Green
**Vial mass: 12.9465g
**Vial + film mass: 13.0751g
**Film mass: 13.0751-12.9465= 0.1286g
*Polymer Film in 10 mL 8 ppm Malachite Green
**Vial mass: 13.0194g
**Vial + film mass: 13.0781g
**Film mass: 13.0781-13.0194= 0.0587g
*Polymer Film in 10 mL 80 ppm Malachite Green
**Vial mass: 12.9579g
**Vial + film mass: 13.0472g
**Film mass: 13.0472-12.9579= 0.0893g
*Polymer Film in 10 mL 200 ppm Malachite Green
**Vial mass: 13.1937g
**Vial + film mass: 13.2917g
**Film mass: 13.2917-13.1937= 0.098g
'''Average polymer film mass: 0.09365g'''<br.>
*Polymer-10% Clay Film in  10 mL 2 ppm Malachite Green
**Vial mass: 13.0053g
**Vial + film mass: 13.0742g
**Film mass: 13.0742-13.0053= 0.0689g
*Polymer-10% Clay Film in  10 mL 8 ppm Malachite Green
**Vial mass: 12.9926g
**Vial + film mass: 13.05845g
**Film mass: 13.75845-12.9926= 0.0.0658
*Polymer-10% Clay Film in 10 mL 80 ppm Malachite Green
**Vial mass: 13.0268g
**Vial + film mass: 13.1033g
**Film mass: 13.1033-13.0268= 0.0765g
*Polymer-10% Clay film in 10 mL 200 ppm Malachite Green
**Vial mass: 13.0753g
**Vial + film mass: 13.1802g
**Film mass: 13.1802-13.0753= 0.1049g
'''Average polymer-10% clay film mass: 0.25404g'''<br.>




Latest revision as of 00:13, 27 September 2017

CHEM 581: Experimental Chemistry Main project page
Previous entry      Next entry

August 29, 2014

Procedures

Completing Film Synthesis

Continued from Wednesday, 8/27/2014<br.> Procedure detailed by Dr Hartings

  • Stir in Sodium Sulfate, 1% HCl, and Sodium Bicarbonate solutions

Beginning New Film Synthesis

Procedure detailed by Dr Hartings

  • Polymer-10% Clay Film
    • 1.0039g PVA and 0.1128g sodium montmorillonite (~1g PVA and ~.1g NaM)
  • Polymer Film
    • 1.0036g PVA (~1g)

Malachite Green Stock Solutions

  • 2.0ppm
    • (2.0ppm)(100mL)=(200.0ppm)*V
    • V=1mL of 200.0ppm solution in 99.0mL water
  • 1.7ppm (25mL)
    • (1.7ppm)(25mL)=(8.0ppm)*V
    • V=5.31mL of 8.0ppm solution in 19.69mL water

Take UV-vis measurements

Soaking Films in Malachite Green Solutions

  • Polymer Film in 10 mL 2 ppm Malachite Green
    • Vial mass: 12.9465g
    • Vial + film mass: 13.0751g
    • Film mass: 13.0751-12.9465= 0.1286g
  • Polymer Film in 10 mL 8 ppm Malachite Green
    • Vial mass: 13.0194g
    • Vial + film mass: 13.0781g
    • Film mass: 13.0781-13.0194= 0.0587g
  • Polymer Film in 10 mL 80 ppm Malachite Green
    • Vial mass: 12.9579g
    • Vial + film mass: 13.0472g
    • Film mass: 13.0472-12.9579= 0.0893g
  • Polymer Film in 10 mL 200 ppm Malachite Green
    • Vial mass: 13.1937g
    • Vial + film mass: 13.2917g
    • Film mass: 13.2917-13.1937= 0.098g

Average polymer film mass: 0.09365g<br.>

  • Polymer-10% Clay Film in 10 mL 2 ppm Malachite Green
    • Vial mass: 13.0053g
    • Vial + film mass: 13.0742g
    • Film mass: 13.0742-13.0053= 0.0689g
  • Polymer-10% Clay Film in 10 mL 8 ppm Malachite Green
    • Vial mass: 12.9926g
    • Vial + film mass: 13.05845g
    • Film mass: 13.75845-12.9926= 0.0.0658
  • Polymer-10% Clay Film in 10 mL 80 ppm Malachite Green
    • Vial mass: 13.0268g
    • Vial + film mass: 13.1033g
    • Film mass: 13.1033-13.0268= 0.0765g
  • Polymer-10% Clay film in 10 mL 200 ppm Malachite Green
    • Vial mass: 13.0753g
    • Vial + film mass: 13.1802g
    • Film mass: 13.1802-13.0753= 0.1049g

Average polymer-10% clay film mass: 0.25404g<br.>



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