User:Madeleine Y. Bee/Notebook/CHEM-581 Experimental Chemistry/2014/09/03: Difference between revisions

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==Entry title==
==September 3, 2014==
* Insert content here...
===Procedures===
====Completing Film Synthesis====
Continued from [http://openwetware.org/wiki/User:Madeleine_Y._Bee/Notebook/CHEM-581_Experimental_Chemistry/2014/08/27 Wednesday, 8/29/2014]<br.>
Procedure detailed by [http://openwetware.org/wiki/User:Matt_Hartings/Notebook/AU_Biomaterials_Design_Lab/2014/08/29 Dr Hartings]
*Stir in Sodium Sulfate, 1% HCl, and Sodium Bicarbonate solutions
 
====Beginning New Film Synthesis====
Procedure detailed by [http://openwetware.org/index.php?title=User:Matt_Hartings/Notebook/AU_Biomaterials_Design_Lab/2014/08/26&action=edit Dr Hartings]
*Polymer-10% Clay Film
**____g PVA and ____g sodium montmorillonite (~1g PVA and ~.1g NaM)
*Polymer Film
**____g PVA (~1g)
 
====UV-vis Measurements====
*Take UV Vis spectra for Malachite green at the following concentrations: 0ppm, 0.20ppm, 0.50ppm, 1.1ppm, 1.4ppm, 1.7ppm, and 2.0ppm
*Construct calibration curve for each of the two absorbance maximums
 
====Equilibrium Measurments====
 
 
====FTIR Measurements====
 
 
====Powder X-ray Diffraction Measurements====
 
 
 
====Differential Scanning Calorimetry Measurments====
 
 





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September 3, 2014

Procedures

Completing Film Synthesis

Continued from Wednesday, 8/29/2014<br.> Procedure detailed by Dr Hartings

  • Stir in Sodium Sulfate, 1% HCl, and Sodium Bicarbonate solutions

Beginning New Film Synthesis

Procedure detailed by Dr Hartings

  • Polymer-10% Clay Film
    • ____g PVA and ____g sodium montmorillonite (~1g PVA and ~.1g NaM)
  • Polymer Film
    • ____g PVA (~1g)

UV-vis Measurements

  • Take UV Vis spectra for Malachite green at the following concentrations: 0ppm, 0.20ppm, 0.50ppm, 1.1ppm, 1.4ppm, 1.7ppm, and 2.0ppm
  • Construct calibration curve for each of the two absorbance maximums

Equilibrium Measurments

FTIR Measurements

Powder X-ray Diffraction Measurements

Differential Scanning Calorimetry Measurments