User:Madeleine Y. Bee/Notebook/Single Molecule Fluorescence/2013/11/13: Difference between revisions
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==November 13, 2013== | ==November 13, 2013== | ||
===Procedures=== | ===Procedures=== | ||
*Synthesis of ZnPPIX | |||
**1:1 molar ratio of Zinc nitrate hexahydrate to Dr Miller's porphyrin | |||
**Dissolve 0.0054g Zn nitrate and 0.0144g porphyrin in 5mL DMF | |||
**Take absorbance measurements every 20 minutes, making 100x dilutions | |||
**Continue heating until absorbance spectra stops changing (80 minutes) | |||
===Data=== | ===Data=== | ||
[[Image:2013_1113_abs_ZnPPIX.PNG]]<br.> | |||
Beer's Law calculations: | |||
[[Image:2013_1113_ZnPPIX_beer's_law_calcs.PNG]] | |||
===Notes=== | ===Notes=== | ||
*In the third, fourth, and fifth samples, it is evident that the spectra stopped changing and the reaction was assumed to be complete | |||
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November 13, 2013Procedures
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