User:Madeleine Y. Bee/Notebook/Single Molecule Fluorescence/2013/11/13

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==November 13, 2013==
==November 13, 2013==
===Procedures===
===Procedures===
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*Synthesis of ZnPPIX
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**1:1 molar ratio of Zinc nitrate hexahydrate to Dr Miller's porphyrin
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**Dissolve 0.0054g Zn nitrate and 0.0144g porphyrin in 5mL DMF
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**Take absorbance measurements every 20 minutes, making 100x dilutions
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**Continue heating until absorbance spectra stops changing (80 minutes)
===Data===
===Data===
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[[Image:2013_1113_abs_ZnPPIX.PNG]]<br.>
===Notes===
===Notes===
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*In the third, fourth, and fifth samples, it is evident that the spectra stopped changing and the reaction was assumed to be complete
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Revision as of 11:11, 13 November 2013

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November 13, 2013

Procedures

  • Synthesis of ZnPPIX
    • 1:1 molar ratio of Zinc nitrate hexahydrate to Dr Miller's porphyrin
    • Dissolve 0.0054g Zn nitrate and 0.0144g porphyrin in 5mL DMF
    • Take absorbance measurements every 20 minutes, making 100x dilutions
    • Continue heating until absorbance spectra stops changing (80 minutes)

Data

Image:2013_1113_abs_ZnPPIX.PNG

Notes

  • In the third, fourth, and fifth samples, it is evident that the spectra stopped changing and the reaction was assumed to be complete


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