User:Matt Hartings/Notebook/AU Biomaterials Design Lab/2014/08/27: Difference between revisions

From OpenWetWare
Jump to navigationJump to search
(fix raw html notebook nav)
 
(3 intermediate revisions by one other user not shown)
Line 2: Line 2:
|-
|-
|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Biomaterials Design Lab</span>
|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Biomaterials Design Lab</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
|style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}}
|-
|-
| colspan="2"|
| colspan="2"|
Line 22: Line 22:
## Stir the solution with constant heating at 75C until the polymer is dissolved and the clay is dispersed (~15 minutes)
## Stir the solution with constant heating at 75C until the polymer is dissolved and the clay is dispersed (~15 minutes)
## Cool the solution to room temperature
## Cool the solution to room temperature
## Add 0.5mL 0.8 wt% glutaraldehyde and 0.5mL 1N HCl to the polymer clay solution.  
## Add 0.5mL 0.8 wt% glutaraldehyde.  
### NOTE: Perform step 4 in the hood
### NOTE: Perform step 4 in the hood
## Stir for an additional 3 minutes to ensure homogeneity
## Stir for an additional 3 minutes to ensure homogeneity
Line 30: Line 30:
## Stir the solution with constant heating at 75C until the polymer is dissolved (~15 minutes)
## Stir the solution with constant heating at 75C until the polymer is dissolved (~15 minutes)
## Cool the solution to room temperature
## Cool the solution to room temperature
## Add 0.5mL 0.8 wt% glutaraldehyde and 0.5mL 1N HCl to the polymer solution.  
## Add 0.5mL 0.8 wt% glutaraldehyde.  
### NOTE: Perform step 4 in the hood
### NOTE: Perform step 4 in the hood
## Stir for an additional 3 minutes to ensure homogeneity
## Stir for an additional 3 minutes to ensure homogeneity

Latest revision as of 00:12, 27 September 2017

Biomaterials Design Lab Main project page
Previous entry      Next entry



Objective

Starting of synthesis for both polymer and polymer-clay films.

Description

Perform the following procedures (1 and 2) in parallel for the start to the synthesis of cross-linked polymer and cross-linked polymer-clay films.

Note: I prepared the starting materials yesterday

  1. Polymer-Clay Films
    1. Add 7mL of water to 1g of 22,000MW polyvinyl alcohol and 0.11g of sodium montmorillonite in a glass vial
    2. Stir the solution with constant heating at 75C until the polymer is dissolved and the clay is dispersed (~15 minutes)
    3. Cool the solution to room temperature
    4. Add 0.5mL 0.8 wt% glutaraldehyde.
      1. NOTE: Perform step 4 in the hood
    5. Stir for an additional 3 minutes to ensure homogeneity
    6. Pour solution into a teflon dish to dry until the next class
  2. Polymer Films
    1. Add 7mL of water to 1g of 22,000MW polyvinyl alcohol in a glass vial
    2. Stir the solution with constant heating at 75C until the polymer is dissolved (~15 minutes)
    3. Cool the solution to room temperature
    4. Add 0.5mL 0.8 wt% glutaraldehyde.
      1. NOTE: Perform step 4 in the hood
    5. Stir for an additional 3 minutes to ensure homogeneity
    6. Pour solution into a teflon dish to dry until the next class

Data

  • Add data and results here...

Notes

This area is for any observations or conclusions that you would like to note.


Use categories like tags. Change the "Course" category to the one corresponding to your course. The "Miscellaneous" tag can be used for particular experiments, as instructed by your professor. Please be sure to change or delete this tag as required so that the categories remain well organized.