User:Megan L. Channell/Notebook/Masters Research/2013/10/03: Difference between revisions

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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
|style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}}
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# Once both fully dissolved, the zinc acetate was added to the organic solution
# Once both fully dissolved, the zinc acetate was added to the organic solution
#Solution stirred for 2.5 hours
#Solution stirred for 2.5 hours
#Filter out solid
*left for the day, so left in the hood
**Next time
#Save ~1 mg of solid
#Put precipitate in 250 mL of DMF and left in hood with watch glass on


==Results==
==Results==

Latest revision as of 23:24, 26 September 2017

Project name Main project page
Next entry

MOF-5 Synthesis

  • Synthesize MOF-5 by using the protocol from FIX THIS (room temp. synthesis of metal-organic frameworks:MOF-5..... Tranchemontagne...)

Protocol

  1. 5.0065 g of terephthalic acid and 8.5 mL of triethylamine dissolved in 400 mL of DMF
  2. 16.881 g of zinc acetate dissolved in 500 mL of DMF
  3. Once both fully dissolved, the zinc acetate was added to the organic solution
  4. Solution stirred for 2.5 hours
  5. Filter out solid
  • left for the day, so left in the hood
    • Next time
  1. Save ~1 mg of solid
  2. Put precipitate in 250 mL of DMF and left in hood with watch glass on

Results


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