User:Megan L. Channell/Notebook/Masters Research/2013/11/21: Difference between revisions

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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
|style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}}
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* The last time I did DSC, it could not finish because there was not enough nitrogen.  I made new samples and re-run them.  The new samples I made were the 0, 0.1, 0.5, 1, 5, and 10% but this time, I added the MOF-5 and the solvent together and sonicated them.  Once they were fully dissolved, I put the PLA in and sonicated them.  Once everything was fully dissolved I poured them into the molds and let them sit overnight.   
* The last time I did DSC, it could not finish because there was not enough nitrogen.  I made new samples and re-run them.  The new samples I made were the 0, 0.1, 0.5, 1, 5, and 10% but this time, I added the MOF-5 and the solvent together and sonicated them.  Once they were fully dissolved, I put the PLA in and sonicated them.  Once everything was fully dissolved I poured them into the molds and let them sit overnight.   


* 0%- .9998 g PLA and 10 mL of diethylamine
#0.1 %, 0.5 %, 1.0 %, 5.0 %, 10 % and 0 % w/v.
##0.1 % - 1.0001 g PLA, 0.001 g MOF-5, 10 mL dichloromethane
##0.5 % - 0.9944 g PLA, 0.0048 g MOF-5, 10 mL dichloromethane
##1.0 % - 0.9903 g PLA, 0.0097 g MOF-5, 10 mL dichloromethane
##5.0 % - 0.509 g PLA, 0.0495 g MOF-5, 10 mL dichloromethane
##10.0 % - 0.8993 g PLA, 0.999 g MOF-5, 10 mL dichloromethane 
##0 % - 0.9998 g PLA, 10 mL dichloromethane
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Latest revision as of 23:36, 26 September 2017

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DSC and new samples

  • The last time I did DSC, it could not finish because there was not enough nitrogen. I made new samples and re-run them. The new samples I made were the 0, 0.1, 0.5, 1, 5, and 10% but this time, I added the MOF-5 and the solvent together and sonicated them. Once they were fully dissolved, I put the PLA in and sonicated them. Once everything was fully dissolved I poured them into the molds and let them sit overnight.
  1. 0.1 %, 0.5 %, 1.0 %, 5.0 %, 10 % and 0 % w/v.
    1. 0.1 % - 1.0001 g PLA, 0.001 g MOF-5, 10 mL dichloromethane
    2. 0.5 % - 0.9944 g PLA, 0.0048 g MOF-5, 10 mL dichloromethane
    3. 1.0 % - 0.9903 g PLA, 0.0097 g MOF-5, 10 mL dichloromethane
    4. 5.0 % - 0.509 g PLA, 0.0495 g MOF-5, 10 mL dichloromethane
    5. 10.0 % - 0.8993 g PLA, 0.999 g MOF-5, 10 mL dichloromethane
    6. 0 % - 0.9998 g PLA, 10 mL dichloromethane


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